Preparation of Hexacoordinated Tris(bidentate) Phosphorus Compounds with 1,3,2-Dioxaphosphorinane Rings. NMR and X-ray Crystallographic Studies of Their Conformation
Тип публикации: Journal Article
Дата публикации: 1999-12-21
scimago Q2
wos Q1
БС1
SJR: 0.737
CiteScore: 6.1
Impact factor: 3.6
ISSN: 00223263, 15206904
PubMed ID:
10813935
Organic Chemistry
Краткое описание
A series of new unstable tris(bidentate) hexacoordinated phosphorus compounds 1 with 1,3,2-dioxaphosphorinane rings was prepared and studied by NMR and X-ray crystallography. The X-ray crystal structures showed that the 1,3,2-dioxaphosphorinane ring adopts different conformations depending on the number and size of substituents at the carbon atom C14. Substituents are deployed around the phosphorus atom in a slightly deformed octahedral structure. Deviations in bond lengths around the phosphorus atom depend on the character of the bonds and the distribution of the negative charge. (1)H and (13)C NMR measurements showed that in solution the flexibility of 1,3,2-dioxaphosphorinane ring depends on the size of substituents at the carbon C14.
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Skowrońska A. et al. Preparation of Hexacoordinated Tris(bidentate) Phosphorus Compounds with 1,3,2-Dioxaphosphorinane Rings. NMR and X-ray Crystallographic Studies of Their Conformation // Journal of Organic Chemistry. 1999. Vol. 65. No. 2. pp. 304-315.
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Skowrońska A., Kowara J., Kaminski R., Bujacz G. D., Wieczorek M. Preparation of Hexacoordinated Tris(bidentate) Phosphorus Compounds with 1,3,2-Dioxaphosphorinane Rings. NMR and X-ray Crystallographic Studies of Their Conformation // Journal of Organic Chemistry. 1999. Vol. 65. No. 2. pp. 304-315.
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TY - JOUR
DO - 10.1021/jo990921w
UR - https://pubs.acs.org/doi/10.1021/jo990921w
TI - Preparation of Hexacoordinated Tris(bidentate) Phosphorus Compounds with 1,3,2-Dioxaphosphorinane Rings. NMR and X-ray Crystallographic Studies of Their Conformation
T2 - Journal of Organic Chemistry
AU - Skowrońska, Aleksandra
AU - Kowara, Jacek
AU - Kaminski, R
AU - Bujacz, Grzegorz D.
AU - Wieczorek, Michal
PY - 1999
DA - 1999/12/21
PB - American Chemical Society (ACS)
SP - 304-315
IS - 2
VL - 65
PMID - 10813935
SN - 0022-3263
SN - 1520-6904
ER -
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@article{1999_Skowrońska,
author = {Aleksandra Skowrońska and Jacek Kowara and R Kaminski and Grzegorz D. Bujacz and Michal Wieczorek},
title = {Preparation of Hexacoordinated Tris(bidentate) Phosphorus Compounds with 1,3,2-Dioxaphosphorinane Rings. NMR and X-ray Crystallographic Studies of Their Conformation},
journal = {Journal of Organic Chemistry},
year = {1999},
volume = {65},
publisher = {American Chemical Society (ACS)},
month = {dec},
url = {https://pubs.acs.org/doi/10.1021/jo990921w},
number = {2},
pages = {304--315},
doi = {10.1021/jo990921w}
}
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Skowrońska, Aleksandra, et al. “Preparation of Hexacoordinated Tris(bidentate) Phosphorus Compounds with 1,3,2-Dioxaphosphorinane Rings. NMR and X-ray Crystallographic Studies of Their Conformation.” Journal of Organic Chemistry, vol. 65, no. 2, Dec. 1999, pp. 304-315. https://pubs.acs.org/doi/10.1021/jo990921w.