Journal of Physical Chemistry B, volume 107, issue 38, pages 10416-10422
Preparation and Characterization of Silver Sulfide Nanocrystals Generated from Silver(I)-Thiolate Polymers
Publication type: Journal Article
Publication date: 2003-08-23
Journal:
Journal of Physical Chemistry B
Q1
Q3
SJR: 0.760
CiteScore: 5.8
Impact factor: 2.8
ISSN: 15206106, 15205207, 10895647
Materials Chemistry
Surfaces, Coatings and Films
Physical and Theoretical Chemistry
Abstract
Silver sulfide nanocrystals have been formed by the conversion of silver thiolate polymers with sodium sulfide in a dual-phase solution preparation. From transmission electron microscopy and laser desorption ionization mass spectrometry, the mean nanocrystalline diameter is estimated to be 5.4 nm. Large-angle X-ray diffraction is qualitatively consistent with the rhombic phase (acanthite) of Ag2S. The removal of the silver thiolate polymer is confirmed by mass spectrometry, and initial results indicate that fractional crystallization may be utilized to separate these large nanocrystalline compounds by their respective core sizes. Optical absorption spectroscopy indicates a band gap of 1.1 eV, which is not shifted appreciably from the bulk value for this direct band gap semiconductor.
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Schaaff T., Rodinone A. J. Preparation and Characterization of Silver Sulfide Nanocrystals Generated from Silver(I)-Thiolate Polymers // Journal of Physical Chemistry B. 2003. Vol. 107. No. 38. pp. 10416-10422.
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Schaaff T., Rodinone A. J. Preparation and Characterization of Silver Sulfide Nanocrystals Generated from Silver(I)-Thiolate Polymers // Journal of Physical Chemistry B. 2003. Vol. 107. No. 38. pp. 10416-10422.
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TY - JOUR
DO - 10.1021/jp034979x
UR - https://doi.org/10.1021/jp034979x
TI - Preparation and Characterization of Silver Sulfide Nanocrystals Generated from Silver(I)-Thiolate Polymers
T2 - Journal of Physical Chemistry B
AU - Schaaff, T.Gregory
AU - Rodinone, Adam J
PY - 2003
DA - 2003/08/23
PB - American Chemical Society (ACS)
SP - 10416-10422
IS - 38
VL - 107
SN - 1520-6106
SN - 1520-5207
SN - 1089-5647
ER -
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@article{2003_Schaaff,
author = {T.Gregory Schaaff and Adam J Rodinone},
title = {Preparation and Characterization of Silver Sulfide Nanocrystals Generated from Silver(I)-Thiolate Polymers},
journal = {Journal of Physical Chemistry B},
year = {2003},
volume = {107},
publisher = {American Chemical Society (ACS)},
month = {aug},
url = {https://doi.org/10.1021/jp034979x},
number = {38},
pages = {10416--10422},
doi = {10.1021/jp034979x}
}
Cite this
MLA
Copy
Schaaff, T.Gregory, and Adam J Rodinone. “Preparation and Characterization of Silver Sulfide Nanocrystals Generated from Silver(I)-Thiolate Polymers.” Journal of Physical Chemistry B, vol. 107, no. 38, Aug. 2003, pp. 10416-10422. https://doi.org/10.1021/jp034979x.