Journal of Physical Chemistry C, volume 111, issue 10, pages 3920-3926

Simultaneous and Rapid Microwave Synthesis of Polyacrylamide−Metal Sulfide (Ag2S, Cu2S, HgS) Nanocomposites

Publication typeJournal Article
Publication date2007-02-20
Quartile SCImago
Q1
Quartile WOS
Q2
Impact factor3.7
ISSN19327447, 19327455
Surfaces, Coatings and Films
Electronic, Optical and Magnetic Materials
Physical and Theoretical Chemistry
General Energy
Abstract
Polyacrylamide−metal sulfide (Ag2S, Cu2S, HgS) nanocomposites with metal sulfide nanoparticles homogeneously dispersed in the polyacrylamide (PAM) matrix have been successfully synthesized using corresponding metal salt, sulfur powder, and acrylamide monomer (AM) in ethylene glycol (EG) by microwave heating. This method is based on the simultaneous formation of metal sulfide nanoparticles and polymerization of the AM, leading to a homogeneous distribution of metal sulfide nanoparticles in PAM matrix without aggregation. EG acts simultaneously as a solvent, a microwave absorber, and a reductant; thus no additional reductant is needed. Another advantage is that no initiator for AM polymerization and no surfactant for the stabilization of these metal sulfide nanoparticles are necessary. The products are characterized by X-ray powder diffraction (XRD), transmission electron microscopy (TEM), Fourier transform infrared (FT-IR), ultraviolet visible (UV−vis) absorption spectra, photoluminescence (PL), thermograv...

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GOST |
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GOST Copy
Zhu J. et al. Simultaneous and Rapid Microwave Synthesis of Polyacrylamide−Metal Sulfide (Ag2S, Cu2S, HgS) Nanocomposites // Journal of Physical Chemistry C. 2007. Vol. 111. No. 10. pp. 3920-3926.
GOST all authors (up to 50) Copy
Zhu J., Zhu Y., Ma M., Yang L., Gao L. Simultaneous and Rapid Microwave Synthesis of Polyacrylamide−Metal Sulfide (Ag2S, Cu2S, HgS) Nanocomposites // Journal of Physical Chemistry C. 2007. Vol. 111. No. 10. pp. 3920-3926.
RIS |
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RIS Copy
TY - JOUR
DO - 10.1021/jp0677851
UR - https://doi.org/10.1021/jp0677851
TI - Simultaneous and Rapid Microwave Synthesis of Polyacrylamide−Metal Sulfide (Ag2S, Cu2S, HgS) Nanocomposites
T2 - Journal of Physical Chemistry C
AU - Yang, Li-Xia
AU - Gao, Lian
AU - Zhu, Jiefang
AU - Zhu, Yingjie
AU - Ma, Mingguo
PY - 2007
DA - 2007/02/20 00:00:00
PB - American Chemical Society (ACS)
SP - 3920-3926
IS - 10
VL - 111
SN - 1932-7447
SN - 1932-7455
ER -
BibTex |
Cite this
BibTex Copy
@article{2007_Zhu,
author = {Li-Xia Yang and Lian Gao and Jiefang Zhu and Yingjie Zhu and Mingguo Ma},
title = {Simultaneous and Rapid Microwave Synthesis of Polyacrylamide−Metal Sulfide (Ag2S, Cu2S, HgS) Nanocomposites},
journal = {Journal of Physical Chemistry C},
year = {2007},
volume = {111},
publisher = {American Chemical Society (ACS)},
month = {feb},
url = {https://doi.org/10.1021/jp0677851},
number = {10},
pages = {3920--3926},
doi = {10.1021/jp0677851}
}
MLA
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MLA Copy
Zhu, Jiefang, et al. “Simultaneous and Rapid Microwave Synthesis of Polyacrylamide−Metal Sulfide (Ag2S, Cu2S, HgS) Nanocomposites.” Journal of Physical Chemistry C, vol. 111, no. 10, Feb. 2007, pp. 3920-3926. https://doi.org/10.1021/jp0677851.
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