Exfoliation and Restacking of Lepidocrocite-type Layered Titanates Studied by Small-Angle X-ray Scattering
Тип публикации: Journal Article
Дата публикации: 2010-11-23
SCImago Q1
WOS Q3
БС1
SJR: 0.82
CiteScore: 5.7
Impact factor: 3.4
ISSN: 19327447, 19327455
Surfaces, Coatings and Films
Electronic, Optical and Magnetic Materials
Physical and Theoretical Chemistry
General Energy
Краткое описание
The exfoliation of the lepidocrocite-type layered titanate K0.8[Ti1.73Li0.27O4] (KLTO) in aqueous solution and the restacking of exfoliated nanosheets was investigated by small-angle X-ray scattering (SAXS). Suspensions with completely exfoliated titania nanosheets of 1 nm thickness were obtained after protonation of KLTO to HTi1.6O3.7 (HTO), followed by addition of tetrabutyl ammonium hydroxide (TBAOH) to a molar ratio TBAOH/HTO = 1. Restacking of nanosheets into small stacks of 2−4 units occurred at TBAOH/HTO ratios of 1.6 or higher. The separation distance between the sheets was found to be reversible and very sensitive to the pH and ionic strength of the solution and increased up to 12 nm. The experimental data indicate that the separation distance between restacked nanosheets scaled with the Debye length of the solution. This suggests that the stacks are organized via electrostatic interactions due to the presence of a diffuse double layer of positively charged ions between the negatively charged nan...
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Besselink R. et al. Exfoliation and Restacking of Lepidocrocite-type Layered Titanates Studied by Small-Angle X-ray Scattering // Journal of Physical Chemistry C. 2010. Vol. 114. No. 49. pp. 21281-21286.
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Besselink R., Stawski T. M., Castricum H. L., Blank D. H., Ten Elshof J. E. Exfoliation and Restacking of Lepidocrocite-type Layered Titanates Studied by Small-Angle X-ray Scattering // Journal of Physical Chemistry C. 2010. Vol. 114. No. 49. pp. 21281-21286.
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TY - JOUR
DO - 10.1021/jp108687q
UR - https://doi.org/10.1021/jp108687q
TI - Exfoliation and Restacking of Lepidocrocite-type Layered Titanates Studied by Small-Angle X-ray Scattering
T2 - Journal of Physical Chemistry C
AU - Besselink, Rogier
AU - Stawski, Tomasz M.
AU - Castricum, Hessel L
AU - Blank, Dave H.A.
AU - Ten Elshof, J. E.
PY - 2010
DA - 2010/11/23
PB - American Chemical Society (ACS)
SP - 21281-21286
IS - 49
VL - 114
SN - 1932-7447
SN - 1932-7455
ER -
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@article{2010_Besselink,
author = {Rogier Besselink and Tomasz M. Stawski and Hessel L Castricum and Dave H.A. Blank and J. E. Ten Elshof},
title = {Exfoliation and Restacking of Lepidocrocite-type Layered Titanates Studied by Small-Angle X-ray Scattering},
journal = {Journal of Physical Chemistry C},
year = {2010},
volume = {114},
publisher = {American Chemical Society (ACS)},
month = {nov},
url = {https://doi.org/10.1021/jp108687q},
number = {49},
pages = {21281--21286},
doi = {10.1021/jp108687q}
}
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MLA
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Besselink, Rogier, et al. “Exfoliation and Restacking of Lepidocrocite-type Layered Titanates Studied by Small-Angle X-ray Scattering.” Journal of Physical Chemistry C, vol. 114, no. 49, Nov. 2010, pp. 21281-21286. https://doi.org/10.1021/jp108687q.
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