Preparation and Electrochemical Performance of Tungstovanadophosphoric Heteropoly Acid and Its Hybrid Materials
Тип публикации: Journal Article
Дата публикации: 2013-02-08
scimago Q1
wos Q3
БС1
SJR: 0.914
CiteScore: 6.2
Impact factor: 3.2
ISSN: 19327447, 19327455
Surfaces, Coatings and Films
Electronic, Optical and Magnetic Materials
Physical and Theoretical Chemistry
General Energy
Краткое описание
Tungstovanadophosphoric heteropoly acid H6PW9V3O40·(13.81 ± 0.13)H2O (abbreviated as PW9V3) has been synthesized by the stepwise acidification and the stepwise addition of element solutions. The crystal structure was determined from single crystal X-ray diffraction. The complex crystallizes in the space group R3m, with a = 16.4374 (9) A, b = 16.4374 (9) A, c = 25.3866 (14) A, α = 90°, β = 90°, γ = 120°, V = 5940.20 A, and Z = 6. The product possesses Keggin structure, and its conductivity was 1.730 × 10–2 S·cm–1 at 26 °C and 75% relative humidity by electrochemical impedance spectroscopy (EIS) measurement. Two conducting systems were prepared with a mixture of as-synthesized PW9V3 and organic polymers [polyvinylpyrrolidone (PVP) or polyethylene glycol (PEG)] at the weight ratio 80:20. The hybrid materials exhibit high proton conductivities with 7.110 × 10–3 and 1.050 × 10–2 S·cm–1 (PW9V3/PEG) at 26 °C and 75% relative humidity, respectively. Their activation energies of proton conduction are 15.23 and 13...
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Tong X. et al. Preparation and Electrochemical Performance of Tungstovanadophosphoric Heteropoly Acid and Its Hybrid Materials // Journal of Physical Chemistry C. 2013. Vol. 117. No. 7. pp. 3258-3263.
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Tong X., Tian N., Wu W., Zhu W., Wu Q., Cao F., Yan W., Yaroslavtsev A. B. Preparation and Electrochemical Performance of Tungstovanadophosphoric Heteropoly Acid and Its Hybrid Materials // Journal of Physical Chemistry C. 2013. Vol. 117. No. 7. pp. 3258-3263.
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TY - JOUR
DO - 10.1021/jp3102223
UR - https://doi.org/10.1021/jp3102223
TI - Preparation and Electrochemical Performance of Tungstovanadophosphoric Heteropoly Acid and Its Hybrid Materials
T2 - Journal of Physical Chemistry C
AU - Tong, Xia
AU - Tian, Naiqin
AU - Wu, Wen
AU - Zhu, Weiming
AU - Wu, Q.
AU - Cao, Fahe
AU - Yan, Wenfu
AU - Yaroslavtsev, A. B.
PY - 2013
DA - 2013/02/08
PB - American Chemical Society (ACS)
SP - 3258-3263
IS - 7
VL - 117
SN - 1932-7447
SN - 1932-7455
ER -
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@article{2013_Tong,
author = {Xia Tong and Naiqin Tian and Wen Wu and Weiming Zhu and Q. Wu and Fahe Cao and Wenfu Yan and A. B. Yaroslavtsev},
title = {Preparation and Electrochemical Performance of Tungstovanadophosphoric Heteropoly Acid and Its Hybrid Materials},
journal = {Journal of Physical Chemistry C},
year = {2013},
volume = {117},
publisher = {American Chemical Society (ACS)},
month = {feb},
url = {https://doi.org/10.1021/jp3102223},
number = {7},
pages = {3258--3263},
doi = {10.1021/jp3102223}
}
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Tong, Xia, et al. “Preparation and Electrochemical Performance of Tungstovanadophosphoric Heteropoly Acid and Its Hybrid Materials.” Journal of Physical Chemistry C, vol. 117, no. 7, Feb. 2013, pp. 3258-3263. https://doi.org/10.1021/jp3102223.
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