Adsorbate Interactions of Paramagnetic Palladium(I) Species in Pd(II)-Exchanged Na−MCM-22 Zeolite
Тип публикации: Journal Article
Дата публикации: 1997-03-01
scimago Q1
wos Q3
БС2
SJR: 0.742
CiteScore: 5.3
Impact factor: 2.9
ISSN: 15206106, 15205207, 10895647
Materials Chemistry
Surfaces, Coatings and Films
Physical and Theoretical Chemistry
Краткое описание
Adsorbate interactions of paramagnetic palladium(I) species in Pd(II)-exchanged Na−MCM-22 zeolite are studied by electron spin resonance (ESR) and electron spin-echo modulation (ESEM) spectroscopies. Oxidation and subsequent evacuation at 825 K of Na−MCM-22 zeolite exchanged with Pd(NH3)4Cl2 results in the formation of a Pd(I) species. Monovalent palladium can be produced in PdNa−MCM-22 material by room temperature hydrogen reduction after dehydration and O2 treatment at high temperature. Addition of hydrogen to PdNa−MCM-22 after dehydration, O2 treatment, and evacuation (activation) is found to increase the concentration of Pd(I) at room temperature and at higher temperature is found to reduce Pd(I) to Pd(0)n (palladium clusters). Adsorption of O2 and H2O to an activated sample containing Pd(I) generates a Pd(II)−O2- species with g⊥ > g∥. Adsorption of CO on an activated sample results in a Pd(I)−(CO)2 complex which partially transforms to Pd(I)−CO on evacuation. Adsorption of ethylene on an activated sa...
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Prakash A., Wasowicz T., Kevan L. Adsorbate Interactions of Paramagnetic Palladium(I) Species in Pd(II)-Exchanged Na−MCM-22 Zeolite // Journal of Physical Chemistry B. 1997. Vol. 101. No. 11. pp. 1985-1993.
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Prakash A., Wasowicz T., Kevan L. Adsorbate Interactions of Paramagnetic Palladium(I) Species in Pd(II)-Exchanged Na−MCM-22 Zeolite // Journal of Physical Chemistry B. 1997. Vol. 101. No. 11. pp. 1985-1993.
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TY - JOUR
DO - 10.1021/jp963455c
UR - https://doi.org/10.1021/jp963455c
TI - Adsorbate Interactions of Paramagnetic Palladium(I) Species in Pd(II)-Exchanged Na−MCM-22 Zeolite
T2 - Journal of Physical Chemistry B
AU - Prakash, A.M.
AU - Wasowicz, Tomasz
AU - Kevan, Larry
PY - 1997
DA - 1997/03/01
PB - American Chemical Society (ACS)
SP - 1985-1993
IS - 11
VL - 101
SN - 1520-6106
SN - 1520-5207
SN - 1089-5647
ER -
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@article{1997_Prakash,
author = {A.M. Prakash and Tomasz Wasowicz and Larry Kevan},
title = {Adsorbate Interactions of Paramagnetic Palladium(I) Species in Pd(II)-Exchanged Na−MCM-22 Zeolite},
journal = {Journal of Physical Chemistry B},
year = {1997},
volume = {101},
publisher = {American Chemical Society (ACS)},
month = {mar},
url = {https://doi.org/10.1021/jp963455c},
number = {11},
pages = {1985--1993},
doi = {10.1021/jp963455c}
}
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Prakash, A.M., et al. “Adsorbate Interactions of Paramagnetic Palladium(I) Species in Pd(II)-Exchanged Na−MCM-22 Zeolite.” Journal of Physical Chemistry B, vol. 101, no. 11, Mar. 1997, pp. 1985-1993. https://doi.org/10.1021/jp963455c.