Influence of Reaction Conditions on the Synthesis of Self-Cross-Linked N-Isopropylacrylamide Microgels
Publication type: Journal Article
Publication date: 2003-05-23
scimago Q1
wos Q2
SJR: 0.763
CiteScore: 6.0
Impact factor: 3.9
ISSN: 07437463, 15205827
Spectroscopy
Electrochemistry
Condensed Matter Physics
General Materials Science
Surfaces and Interfaces
Abstract
We report systematic investigations of the reaction conditions necessary for the production of self-cross-linked poly(N-isopropylacrylamide) (PNIPAM) microgel particles. Reaction temperatures (Tsyn) ranging from 40 to 90 °C and various monomer (CNIPAM) and initiator (CKPS) concentrations were investigated. Laser light scattering was used to characterize the resultant gel particles at 25 and 40 °C, below and above the phase transition temperature of PNIPAM. By comparing the molar masses measured at these two temperatures, well-defined ranges of Tsyn, CNIPAM, and CKPS were found in which the polymer chains were well self-cross-linked and formed gel networks. Variations in the size and solid density as a function of these parameters are also discussed.
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101
Total citations:
101
Citations from 2025:
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(2.97%)
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GOST
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Gao J., Frisken B. J. Influence of Reaction Conditions on the Synthesis of Self-Cross-Linked N-Isopropylacrylamide Microgels // Langmuir. 2003. Vol. 19. No. 13. pp. 5217-5222.
GOST all authors (up to 50)
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Gao J., Frisken B. J. Influence of Reaction Conditions on the Synthesis of Self-Cross-Linked N-Isopropylacrylamide Microgels // Langmuir. 2003. Vol. 19. No. 13. pp. 5217-5222.
Cite this
RIS
Copy
TY - JOUR
DO - 10.1021/la034207s
UR - https://doi.org/10.1021/la034207s
TI - Influence of Reaction Conditions on the Synthesis of Self-Cross-Linked N-Isopropylacrylamide Microgels
T2 - Langmuir
AU - Gao, Jun
AU - Frisken, Barbara J
PY - 2003
DA - 2003/05/23
PB - American Chemical Society (ACS)
SP - 5217-5222
IS - 13
VL - 19
SN - 0743-7463
SN - 1520-5827
ER -
Cite this
BibTex (up to 50 authors)
Copy
@article{2003_Gao,
author = {Jun Gao and Barbara J Frisken},
title = {Influence of Reaction Conditions on the Synthesis of Self-Cross-Linked N-Isopropylacrylamide Microgels},
journal = {Langmuir},
year = {2003},
volume = {19},
publisher = {American Chemical Society (ACS)},
month = {may},
url = {https://doi.org/10.1021/la034207s},
number = {13},
pages = {5217--5222},
doi = {10.1021/la034207s}
}
Cite this
MLA
Copy
Gao, Jun, and Barbara J Frisken. “Influence of Reaction Conditions on the Synthesis of Self-Cross-Linked N-Isopropylacrylamide Microgels.” Langmuir, vol. 19, no. 13, May. 2003, pp. 5217-5222. https://doi.org/10.1021/la034207s.