β-Cyclodextrin Dimers Linked through Their Secondary Faces with Rigid Spacer Arms as Hosts for Bile Salts
Publication type: Journal Article
Publication date: 2011-07-12
scimago Q1
wos Q2
SJR: 0.763
CiteScore: 6.0
Impact factor: 3.9
ISSN: 07437463, 15205827
PubMed ID:
21702438
Spectroscopy
Electrochemistry
Condensed Matter Physics
General Materials Science
Surfaces and Interfaces
Abstract
A convenient synthesis of β-cyclodextrin dimers in which the two cyclodextrin units are linked by rigid tethers of relatively short length through their secondary sides is reported. Compounds hexa-2,4-diynediyl- and 1,4-phenylenediethyne-briged β-cyclodextrin dimers are obtained in good yields from mono-2-O-propargyl-β-cyclodextrin through Pd-mediated oxidative homo- and heterocoupling reactions. Isothermal titration calorimetry and NMR spectroscopy (PGSE and 2D-ROESY) are used to determine the thermodynamic parameters (K, ΔH, and TΔS°) for the complexation of such β-cyclodextrin dimers with sodium cholate, deoxycholate, and chenodeoxycholate as well as to estimate the size of the supramolecular structures. The binding of bile salts is enhanced relative to that of native β-cyclodextrin. Although chenodeoxycholate salt binds in a 1:1 fashion, cholate and deoxycholate salts bind in a 1:2 sequential mode.
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GOST
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Manuel Casas-Solvas J. et al. β-Cyclodextrin Dimers Linked through Their Secondary Faces with Rigid Spacer Arms as Hosts for Bile Salts // Langmuir. 2011. Vol. 27. No. 16. pp. 9729-9737.
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Manuel Casas-Solvas J., Quesada Soriano I., Carreño Gázquez D., Giménez Martínez J. J., García-Fuentes L., Vargas-Berenguel A. β-Cyclodextrin Dimers Linked through Their Secondary Faces with Rigid Spacer Arms as Hosts for Bile Salts // Langmuir. 2011. Vol. 27. No. 16. pp. 9729-9737.
Cite this
RIS
Copy
TY - JOUR
DO - 10.1021/la201180u
UR - https://doi.org/10.1021/la201180u
TI - β-Cyclodextrin Dimers Linked through Their Secondary Faces with Rigid Spacer Arms as Hosts for Bile Salts
T2 - Langmuir
AU - Manuel Casas-Solvas, Juan
AU - Quesada Soriano, Indalecio
AU - Carreño Gázquez, Dolores
AU - Giménez Martínez, Juan J
AU - García-Fuentes, Luis
AU - Vargas-Berenguel, A.
PY - 2011
DA - 2011/07/12
PB - American Chemical Society (ACS)
SP - 9729-9737
IS - 16
VL - 27
PMID - 21702438
SN - 0743-7463
SN - 1520-5827
ER -
Cite this
BibTex (up to 50 authors)
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@article{2011_Manuel Casas-Solvas,
author = {Juan Manuel Casas-Solvas and Indalecio Quesada Soriano and Dolores Carreño Gázquez and Juan J Giménez Martínez and Luis García-Fuentes and A. Vargas-Berenguel},
title = {β-Cyclodextrin Dimers Linked through Their Secondary Faces with Rigid Spacer Arms as Hosts for Bile Salts},
journal = {Langmuir},
year = {2011},
volume = {27},
publisher = {American Chemical Society (ACS)},
month = {jul},
url = {https://doi.org/10.1021/la201180u},
number = {16},
pages = {9729--9737},
doi = {10.1021/la201180u}
}
Cite this
MLA
Copy
Manuel Casas-Solvas, Juan, et al. “β-Cyclodextrin Dimers Linked through Their Secondary Faces with Rigid Spacer Arms as Hosts for Bile Salts.” Langmuir, vol. 27, no. 16, Jul. 2011, pp. 9729-9737. https://doi.org/10.1021/la201180u.