Synthesis of Hydroxy-Telechelic Poly(methyl acrylate) and Polystyrene by Atom Transfer Radical Coupling
Тип публикации: Journal Article
Дата публикации: 2004-12-01
SCImago Q1
Tоп 10% SCImago
WOS Q1
БС1
SJR: 1.257
CiteScore: 9
Impact factor: 5.2
ISSN: 00249297, 15205835
Materials Chemistry
Organic Chemistry
Inorganic Chemistry
Polymers and Plastics
Краткое описание
Hydroxy-terminated poly(methyl acrylate) (HO-PMABr) and polystyrene (HO-PStBr) were synthesized by atom transfer radical polymerization (ATRP) using a HO-functionalized initiator. These HO-functional polymers were further employed in an atom transfer radical coupling (ATRC) reaction in the presence of a zerovalent metal forming hydroxy-telechelic poly(methyl acrylate) (HO-PMA-OH) and polystyrene (HO-PSt-OH). In ATRC process macroradicals, generated in situ by an atom transfer radical equilibrium, take part in bimolecular termination reactions in the presence of a reducing agent, such as nanosize copper. The coupling of hydroxy-terminated PSt was fast; after 3 h more than 95% of polymeric chains being reacted. Under similar ATRC conditions, the coupling of poly(methyl acrylate) was slow since the ATRP equilibrium constant, and consequently radical concentration, is much smaller than those of polystyrene. This difficulty was overcome by introducing small amounts of St in the ATRC of polyacrylate. The acryla...
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ГОСТ
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Sarbu T. et al. Synthesis of Hydroxy-Telechelic Poly(methyl acrylate) and Polystyrene by Atom Transfer Radical Coupling // Macromolecules. 2004. Vol. 37. No. 26. pp. 9694-9700.
ГОСТ со всеми авторами (до 50)
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Sarbu T., Lin K. Y., Spanswick J., Gil R. A., Siegwart D. J., Matyjaszewski K. Synthesis of Hydroxy-Telechelic Poly(methyl acrylate) and Polystyrene by Atom Transfer Radical Coupling // Macromolecules. 2004. Vol. 37. No. 26. pp. 9694-9700.
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TY - JOUR
DO - 10.1021/ma0484375
UR - https://doi.org/10.1021/ma0484375
TI - Synthesis of Hydroxy-Telechelic Poly(methyl acrylate) and Polystyrene by Atom Transfer Radical Coupling
T2 - Macromolecules
AU - Sarbu, Traian
AU - Lin, Koon Yee
AU - Spanswick, James
AU - Gil, Roberto A.
AU - Siegwart, Daniel J
AU - Matyjaszewski, Krzysztof
PY - 2004
DA - 2004/12/01
PB - American Chemical Society (ACS)
SP - 9694-9700
IS - 26
VL - 37
SN - 0024-9297
SN - 1520-5835
ER -
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BibTex (до 50 авторов)
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@article{2004_Sarbu,
author = {Traian Sarbu and Koon Yee Lin and James Spanswick and Roberto A. Gil and Daniel J Siegwart and Krzysztof Matyjaszewski},
title = {Synthesis of Hydroxy-Telechelic Poly(methyl acrylate) and Polystyrene by Atom Transfer Radical Coupling},
journal = {Macromolecules},
year = {2004},
volume = {37},
publisher = {American Chemical Society (ACS)},
month = {dec},
url = {https://doi.org/10.1021/ma0484375},
number = {26},
pages = {9694--9700},
doi = {10.1021/ma0484375}
}
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MLA
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Sarbu, Traian, et al. “Synthesis of Hydroxy-Telechelic Poly(methyl acrylate) and Polystyrene by Atom Transfer Radical Coupling.” Macromolecules, vol. 37, no. 26, Dec. 2004, pp. 9694-9700. https://doi.org/10.1021/ma0484375.
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