ACS Nano, volume 6, issue 3, pages 2833-2843
Controlled Synthesis of Compositionally Tunable Ternary PbSexS1–x as Well as Binary PbSe and PbS Nanowires
Publication type: Journal Article
Publication date: 2012-02-24
General Physics and Astronomy
General Materials Science
General Engineering
Abstract
High-quality compositionally tunable ternary PbSe(x)S(1-x) (x = 0.23, 0.39, 0.49, 0.68, and 0.90) nanowires (NWs) and their binary analogues have been grown using solution-liquid-solid growth with lead(II) diethyldithiocarbamate, Pb(S(2)CNEt(2))(2), and lead(II) imido(bis(selenodiisopropylphosphinate)), Pb((SeP(i)Pr(2))(2)N)(2), as single-source precursors. The alloyed nature of PbSe(x)S(1-x) wires was confirmed using ensemble X-ray diffraction and energy dispersive X-ray spectroscopy (EDXS). Single NW EDXS line scans taken along the length of individual wires show no compositional gradients. NW compositions were independently confirmed using inductively coupled plasma atomic emission spectroscopy. Slight stoichiometric deviations occur but never exceed 13.3% of the expected composition, based on the amount of introduced precursor. In all cases, resulting nanowires have been characterized using transmission electron microscopy. Mean diameters are between 9 and 15 nm with accompanying lengths that range from 4 to 10 μm. Associated selected area electron diffraction patterns indicate that the PbSe(x)S(1-x), PbSe, and PbS NWs all possess the same <002> growth direction, with diffraction patterns consistent with an underlying rock salt crystal structure.
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Citations by publishers
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Taylor & Francis
1 publication, 2.08%
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Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii
1 publication, 2.08%
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Onicha A. C. et al. Controlled Synthesis of Compositionally Tunable Ternary PbSexS1–x as Well as Binary PbSe and PbS Nanowires // ACS Nano. 2012. Vol. 6. No. 3. pp. 2833-2843.
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Onicha A. C., Petchsang N., Kosel T. H., Kuno M. Controlled Synthesis of Compositionally Tunable Ternary PbSexS1–x as Well as Binary PbSe and PbS Nanowires // ACS Nano. 2012. Vol. 6. No. 3. pp. 2833-2843.
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TY - JOUR
DO - 10.1021/nn300373w
UR - https://doi.org/10.1021/nn300373w
TI - Controlled Synthesis of Compositionally Tunable Ternary PbSexS1–x as Well as Binary PbSe and PbS Nanowires
T2 - ACS Nano
AU - Onicha, Anthony C
AU - Kosel, Thomas H.
AU - Petchsang, N.
AU - Kuno, Masaru
PY - 2012
DA - 2012/02/24 00:00:00
PB - American Chemical Society (ACS)
SP - 2833-2843
IS - 3
VL - 6
SN - 1936-0851
SN - 1936-086X
ER -
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@article{2012_Onicha,
author = {Anthony C Onicha and Thomas H. Kosel and N. Petchsang and Masaru Kuno},
title = {Controlled Synthesis of Compositionally Tunable Ternary PbSexS1–x as Well as Binary PbSe and PbS Nanowires},
journal = {ACS Nano},
year = {2012},
volume = {6},
publisher = {American Chemical Society (ACS)},
month = {feb},
url = {https://doi.org/10.1021/nn300373w},
number = {3},
pages = {2833--2843},
doi = {10.1021/nn300373w}
}
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Onicha, Anthony C., et al. “Controlled Synthesis of Compositionally Tunable Ternary PbSexS1–x as Well as Binary PbSe and PbS Nanowires.” ACS Nano, vol. 6, no. 3, Feb. 2012, pp. 2833-2843. https://doi.org/10.1021/nn300373w.