Organic Letters

, том 16 , издание 7 , страницы 1888-1891

Carbonylative Suzuki Couplings of Aryl Bromides with Boronic Acid Derivatives under Base-Free Conditions

Тип публикации: Journal Article

Дата публикации: 2014-03-17

American Chemical Society (ACS)

Organic Letters

scimago Q1

wos Q1

БС1

SJR: 1.235

CiteScore: 8.7

Impact factor: 5.0

ISSN: 15237060, 15237052

DOI: 10.1021/ol5003362

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PubMed ID: 24635142

Organic Chemistry

Biochemistry

Physical and Theoretical Chemistry

Краткое описание

The carbonylative Suzuki-Miyaura reaction between aryl bromides and arylboronic acid equivalents is herein reported, using base-free conditions and a limited excess of carbon monoxide generated ex situ from stable CO-precursors. Under these conditions, unsymmetrical biaryl ketones were obtained in modest to excellent yields. This method was adapted to the synthesis of the triglyceride and cholesterol regulator drug, fenofibrate, and its (13)C-labeled derivative in good yields from the appropriate CO-precursor.

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Тихомиров Александр

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д.х.н., доц.

60 публикаций, 976 цитирований

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Российский химико-технологический университет имени Д. И. Менделеева

Научно-исследовательский институт по изысканию новых антибиотиков имени Г.Ф. Гаузе

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Медицинская химия

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Литвинова Валерия

к.х.н.

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Научно-исследовательский институт по изысканию новых антибиотиков имени Г.Ф. Гаузе

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Антибиотики

Органический синтез

Синтез биологически активных веществ

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Раевский Алексей

49 публикаций, 251 цитирование

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Bjerglund K. M. et al. Carbonylative Suzuki Couplings of Aryl Bromides with Boronic Acid Derivatives under Base-Free Conditions // Organic Letters. 2014. Vol. 16. No. 7. pp. 1888-1891.

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Bjerglund K. M., Skrydstrup T., Molander G. A. Carbonylative Suzuki Couplings of Aryl Bromides with Boronic Acid Derivatives under Base-Free Conditions // Organic Letters. 2014. Vol. 16. No. 7. pp. 1888-1891.

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TY - JOUR

DO - 10.1021/ol5003362

UR - https://doi.org/10.1021/ol5003362

TI - Carbonylative Suzuki Couplings of Aryl Bromides with Boronic Acid Derivatives under Base-Free Conditions

T2 - Organic Letters

AU - Bjerglund, Klaus M

AU - Skrydstrup, Troels

AU - Molander, Gary A.

PY - 2014

DA - 2014/03/17

PB - American Chemical Society (ACS)

SP - 1888-1891

IS - 7

VL - 16

PMID - 24635142

SN - 1523-7060

SN - 1523-7052

ER -

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@article{2014_Bjerglund,

author = {Klaus M Bjerglund and Troels Skrydstrup and Gary A. Molander},

title = {Carbonylative Suzuki Couplings of Aryl Bromides with Boronic Acid Derivatives under Base-Free Conditions},

journal = {Organic Letters},

year = {2014},

volume = {16},

publisher = {American Chemical Society (ACS)},

month = {mar},

url = {https://doi.org/10.1021/ol5003362},

number = {7},

pages = {1888--1891},

doi = {10.1021/ol5003362}

}

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Bjerglund, Klaus M., et al. “Carbonylative Suzuki Couplings of Aryl Bromides with Boronic Acid Derivatives under Base-Free Conditions.” Organic Letters, vol. 16, no. 7, Mar. 2014, pp. 1888-1891. https://doi.org/10.1021/ol5003362.