Organic Letters

, том 9 , издание 22 , страницы 4491-4494

SmCl₃-Catalyzed C-Acylation of 1,3-Dicarbonyl Compounds and Malononitrile

Тип публикации: Journal Article

Дата публикации: 2007-09-29

American Chemical Society (ACS)

Organic Letters

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SJR: 1.235

CiteScore: 8.7

Impact factor: 5

ISSN: 15237060, 15237052

DOI: 10.1021/ol701961z

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PubMed ID: 17902683

Organic Chemistry

Biochemistry

Physical and Theoretical Chemistry

Краткое описание

A recyclable, convenient, and efficient catalytic system for C-acylation of 1,3-dicarbonyl compounds and malononitrile with acid chlorides has been developed, giving moderate to excellent yields under mild conditions. This is the first catalytic example of such reactions. In addition, by applying this protocol as the key step, 3,5-disubstituted-1H-pyrazole-4-carboxylate can easily be synthesized in high yields in a one-pot procedure.

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Shen Q. et al. SmCl3-Catalyzed C-Acylation of 1,3-Dicarbonyl Compounds and Malononitrile // Organic Letters. 2007. Vol. 9. No. 22. pp. 4491-4494.

ГОСТ со всеми авторами (до 50) Скопировать

Shen Q., Huang W., Wang J., Zhou X. SmCl3-Catalyzed C-Acylation of 1,3-Dicarbonyl Compounds and Malononitrile // Organic Letters. 2007. Vol. 9. No. 22. pp. 4491-4494.

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TY - JOUR

DO - 10.1021/ol701961z

UR - https://doi.org/10.1021/ol701961z

TI - SmCl3-Catalyzed C-Acylation of 1,3-Dicarbonyl Compounds and Malononitrile

T2 - Organic Letters

AU - Shen, Quansheng

AU - Huang, Wen

AU - Wang, Jialiang

AU - Zhou, Xigeng

PY - 2007

DA - 2007/09/29

PB - American Chemical Society (ACS)

SP - 4491-4494

IS - 22

VL - 9

PMID - 17902683

SN - 1523-7060

SN - 1523-7052

ER -

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@article{2007_Shen,

author = {Quansheng Shen and Wen Huang and Jialiang Wang and Xigeng Zhou},

title = {SmCl3-Catalyzed C-Acylation of 1,3-Dicarbonyl Compounds and Malononitrile},

journal = {Organic Letters},

year = {2007},

volume = {9},

publisher = {American Chemical Society (ACS)},

month = {sep},

url = {https://doi.org/10.1021/ol701961z},

number = {22},

pages = {4491--4494},

doi = {10.1021/ol701961z}

}

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Shen, Quansheng, et al. “SmCl3-Catalyzed C-Acylation of 1,3-Dicarbonyl Compounds and Malononitrile.” Organic Letters, vol. 9, no. 22, Sep. 2007, pp. 4491-4494. https://doi.org/10.1021/ol701961z.