Air- and Moisture-Stable Cyclopalladated Complexes as Efficient Catalysts for Suzuki-Miyaura Coupling Reaction
Тип публикации: Journal Article
Дата публикации: 2005-02-09
scimago Q2
wos Q1
БС1
SJR: 0.676
CiteScore: 5.1
Impact factor: 2.9
ISSN: 02767333, 15206041
Organic Chemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Краткое описание
A series of cylcopalladated complexes containing a six-membered chelating ring with the general formula [Pd(Cl)(k2N,C-CH2C6H2(Me)2CHNAr)]2 [where Ar = 2,6-(Me)2C6H3− (3a); 2,6-(iPr)2C6H3− (3b)] and the related phosphine-substituted species [PdCl(k2N,C-CH2C6H2(Me)2CHNAr)(PR3)] [Ar = 2,6-(Me)2C6H3−, R = Cy (5a); Ar = 2,6-(iPr)2C6H3, R = Cy (5b); Ar = 2,6-(Me)2C6H3−, R = Ph (5c); Ar = 2,6-(iPr)2C6H3−, R = Ph (5d)] have been synthesized. In addition, an ortho-metalated complex [PdCl(k2N,C-C6H4CHN(2,6-iPr2C6H3))(PCy3)] (7) was prepared by a similar manner. Crystal structures of 3a, 5b,c, and 7 have been determined. The use of these palladium complexes as catalysts for Suzuki−Miyaura coupling reaction of aryl halides with arylboronic acids in ethanol solution was examined. It is found that this series of palladacycles are considerably active under aerobic conditions. Typically, the best activity (TON ≈ 106) is seen with 3a,b in the coupling reaction of aryl bromide with phenylboronic acid. However, a TEM study ...
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Chen C. L. et al. Air- and Moisture-Stable Cyclopalladated Complexes as Efficient Catalysts for Suzuki-Miyaura Coupling Reaction // Organometallics. 2005. Vol. 24. No. 6. pp. 1075-1081.
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Chen C. L., Liu Y., Peng S. T. J., Liu S. Air- and Moisture-Stable Cyclopalladated Complexes as Efficient Catalysts for Suzuki-Miyaura Coupling Reaction // Organometallics. 2005. Vol. 24. No. 6. pp. 1075-1081.
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TY - JOUR
DO - 10.1021/om049125t
UR - https://doi.org/10.1021/om049125t
TI - Air- and Moisture-Stable Cyclopalladated Complexes as Efficient Catalysts for Suzuki-Miyaura Coupling Reaction
T2 - Organometallics
AU - Chen, Chuan Lin
AU - Liu, Yi-Hung
AU - Peng, S. T. J.
AU - Liu, Shiuh-Inn
PY - 2005
DA - 2005/02/09
PB - American Chemical Society (ACS)
SP - 1075-1081
IS - 6
VL - 24
SN - 0276-7333
SN - 1520-6041
ER -
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@article{2005_Chen,
author = {Chuan Lin Chen and Yi-Hung Liu and S. T. J. Peng and Shiuh-Inn Liu},
title = {Air- and Moisture-Stable Cyclopalladated Complexes as Efficient Catalysts for Suzuki-Miyaura Coupling Reaction},
journal = {Organometallics},
year = {2005},
volume = {24},
publisher = {American Chemical Society (ACS)},
month = {feb},
url = {https://doi.org/10.1021/om049125t},
number = {6},
pages = {1075--1081},
doi = {10.1021/om049125t}
}
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MLA
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Chen, Chuan Lin, et al. “Air- and Moisture-Stable Cyclopalladated Complexes as Efficient Catalysts for Suzuki-Miyaura Coupling Reaction.” Organometallics, vol. 24, no. 6, Feb. 2005, pp. 1075-1081. https://doi.org/10.1021/om049125t.