Catalytic Cycloalumination for the Synthesis of Norbornane-Annulated Phospholanes
Publication type: Journal Article
Publication date: 2014-12-31
scimago Q2
wos Q1
SJR: 0.676
CiteScore: 5.1
Impact factor: 2.9
ISSN: 02767333, 15206041
Organic Chemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
An effective one-pot method for the synthesis of polycyclic phospholanes by in situ reaction of dichlorophosphines (RPCl2, where R = Ph, t-Bu, Me) with norbornane-annulated aluminacyclopentanes was obtained by catalytic cycloalumination of norbornenes. Oxidation of phospholanes gave the corresponding polycyclic phospholane 3-oxides (3-sulfides). The molybdenum complex L2Mo(CO)4 (L = 3-phenyl-3-phosphatricyclo[5.2.1.02,6]decane) was prepared for the first time by the reaction of 3-phenyl-3-phosphatricyclo[5.2.1.02,6]decane with molybdenum hexacarbonyl. The structures of the obtained compounds were confirmed by X-ray diffraction and multinuclear 1H, 13C, and 31P NMR spectroscopy.
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Total citations:
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Citations from 2024:
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(4.55%)
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GOST
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D'yakonov V. A. et al. Catalytic Cycloalumination for the Synthesis of Norbornane-Annulated Phospholanes // Organometallics. 2014. Vol. 34. No. 1. pp. 221-228.
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D'yakonov V. A., Makhamatkhanova A. L., Dilmukhametova L. K., Agliullina R. A., Tyumkina T. V., Dzhemilev U. M. Catalytic Cycloalumination for the Synthesis of Norbornane-Annulated Phospholanes // Organometallics. 2014. Vol. 34. No. 1. pp. 221-228.
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RIS
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TY - JOUR
DO - 10.1021/om5010463
UR - https://doi.org/10.1021/om5010463
TI - Catalytic Cycloalumination for the Synthesis of Norbornane-Annulated Phospholanes
T2 - Organometallics
AU - D'yakonov, Vladimir A
AU - Makhamatkhanova, Alevtina L
AU - Dilmukhametova, Leisan K
AU - Agliullina, Rina A
AU - Tyumkina, Tatyana V
AU - Dzhemilev, Usein M
PY - 2014
DA - 2014/12/31
PB - American Chemical Society (ACS)
SP - 221-228
IS - 1
VL - 34
SN - 0276-7333
SN - 1520-6041
ER -
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BibTex (up to 50 authors)
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@article{2014_D'yakonov,
author = {Vladimir A D'yakonov and Alevtina L Makhamatkhanova and Leisan K Dilmukhametova and Rina A Agliullina and Tatyana V Tyumkina and Usein M Dzhemilev},
title = {Catalytic Cycloalumination for the Synthesis of Norbornane-Annulated Phospholanes},
journal = {Organometallics},
year = {2014},
volume = {34},
publisher = {American Chemical Society (ACS)},
month = {dec},
url = {https://doi.org/10.1021/om5010463},
number = {1},
pages = {221--228},
doi = {10.1021/om5010463}
}
Cite this
MLA
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D'yakonov, Vladimir A., et al. “Catalytic Cycloalumination for the Synthesis of Norbornane-Annulated Phospholanes.” Organometallics, vol. 34, no. 1, Dec. 2014, pp. 221-228. https://doi.org/10.1021/om5010463.