Crown Ether Palladacycles as Metalloligands: Suitable Precursors for Tetranuclear Mixed Transition/Non-Transition Metal Complexes
Publication type: Journal Article
Publication date: 2009-11-06
scimago Q2
wos Q1
SJR: 0.676
CiteScore: 5.1
Impact factor: 2.9
ISSN: 02767333, 15206041
Organic Chemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
Reaction of Pd(OAc)2 with the Schiff base ligands 2,3,4-(MeO)3C6H2C(H)═N-[9,10-(C8H16O5)C6H3] (a) and 2,3,4-(MeO)3C6H2C(H)═N[9,10-(C10H20O6)C6H3] (b) leads to the cyclometalated compounds [Pd{2,3,4-(MeO)3C6HC(H)═N-[9,10-(C8H16O5)C6H3]-C6,N}(μ-O2CMe)]2 (1a) and [Pd{2,3,4-(MeO)3C6HC(H)═N[9,10-(C10H20O6)C6H3]-C6,N}(μ-O2CMe)]2 (1b), respectively, via C−H activation. The metathesis reaction of 1a with aqueous tetrabutylammonium chloride gave the corresponding cyclopalladated dimer with bridging chloride ligands, 2a. Treatment of the dimer compounds with NaClO4, KClO4, NH4PF6, Pb(SCN)2, RbClO4, and Ba(ClO4)2 gave the corresponding products in which the cation (Na+, K+, NH4+, Pb2+, Rb+, Ba2+) was coordinated to the crown ether moiety. The structures of compounds 1a and 6a (a complex with one Na+ cation coordinated to each crown ether group) have been determined by X-ray single-crystal diffraction analysis.
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Castro-Juiz S. et al. Crown Ether Palladacycles as Metalloligands: Suitable Precursors for Tetranuclear Mixed Transition/Non-Transition Metal Complexes // Organometallics. 2009. Vol. 28. No. 23. pp. 6657-6665.
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Castro-Juiz S., Fernández A., López-Torres M., Vázquez-Garcı́a D., Suárez A. J., Andrade Vila J. H., Fernández J. M. Crown Ether Palladacycles as Metalloligands: Suitable Precursors for Tetranuclear Mixed Transition/Non-Transition Metal Complexes // Organometallics. 2009. Vol. 28. No. 23. pp. 6657-6665.
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TY - JOUR
DO - 10.1021/om900390a
UR - https://doi.org/10.1021/om900390a
TI - Crown Ether Palladacycles as Metalloligands: Suitable Precursors for Tetranuclear Mixed Transition/Non-Transition Metal Complexes
T2 - Organometallics
AU - Castro-Juiz, Samuel
AU - Fernández, Alberto
AU - López-Torres, Margarita
AU - Vázquez-Garcı́a, Digna
AU - Suárez, Antonio J
AU - Andrade Vila, José Henrique
AU - Fernández, Jesús Martín
PY - 2009
DA - 2009/11/06
PB - American Chemical Society (ACS)
SP - 6657-6665
IS - 23
VL - 28
SN - 0276-7333
SN - 1520-6041
ER -
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@article{2009_Castro-Juiz,
author = {Samuel Castro-Juiz and Alberto Fernández and Margarita López-Torres and Digna Vázquez-Garcı́a and Antonio J Suárez and José Henrique Andrade Vila and Jesús Martín Fernández},
title = {Crown Ether Palladacycles as Metalloligands: Suitable Precursors for Tetranuclear Mixed Transition/Non-Transition Metal Complexes},
journal = {Organometallics},
year = {2009},
volume = {28},
publisher = {American Chemical Society (ACS)},
month = {nov},
url = {https://doi.org/10.1021/om900390a},
number = {23},
pages = {6657--6665},
doi = {10.1021/om900390a}
}
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Castro-Juiz, Samuel, et al. “Crown Ether Palladacycles as Metalloligands: Suitable Precursors for Tetranuclear Mixed Transition/Non-Transition Metal Complexes.” Organometallics, vol. 28, no. 23, Nov. 2009, pp. 6657-6665. https://doi.org/10.1021/om900390a.