Springer Nature
Journal of Chemical Crystallography
,  том 30 ,  издание 11 ,  страницы 721-726

Hydrothermal synthesis and X-ray structure: A reduced titanic molybdenum(V) phosphate (NH3CH2CH2NH2)5Na [Ti2Mo12O30(PO4)(HPO4)4(H2PO4)3]⋅6H2O

Тип публикации: Journal Article
Дата публикации: 2000-01-01
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ISSN: 10741542, 15728854
General Chemistry
Condensed Matter Physics
Краткое описание
A novel titanic molybdenum(V) phosphate (NH3CH2CH2NH2)5Na [Ti2Mo12O30(PO4) (HPO4)4(H2PO4)3]⋅6H2O crystallizes in the triclinic space group P1 with a = 12.057(3) Å, b = 14.668(2) Å, c = 21.2680(10) Å, α = 80.840(10)°, β = 82.960(10)°, γ = 76.65(2)°, and D c = 2.707 g cm−3 for Z = 2, Refinement based on 12,037 observed reflections led to R = 0.0609. The result of single crystal x-ray diffraction revealed the presence of a tunnel and two crystallographically independent clusters in the solid state structure. The plane layers in its solid-state structure are interconnected in-sheet (axial) through multipoint hydrogen bonding between the ethylenediamine nitrogen atoms and the cluster oxygen atoms.
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Xu L. et al. Hydrothermal synthesis and X-ray structure: A reduced titanic molybdenum(V) phosphate (NH3CH2CH2NH2)5Na [Ti2Mo12O30(PO4)(HPO4)4(H2PO4)3]⋅6H2O // Journal of Chemical Crystallography. 2000. Vol. 30. No. 11. pp. 721-726.
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Xu L., Sun Y., WANG E., Li M., Hu C., Huang R. Hydrothermal synthesis and X-ray structure: A reduced titanic molybdenum(V) phosphate (NH3CH2CH2NH2)5Na [Ti2Mo12O30(PO4)(HPO4)4(H2PO4)3]⋅6H2O // Journal of Chemical Crystallography. 2000. Vol. 30. No. 11. pp. 721-726.
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TY - JOUR
DO - 10.1023/a:1012298127786
UR - https://doi.org/10.1023/a:1012298127786
TI - Hydrothermal synthesis and X-ray structure: A reduced titanic molybdenum(V) phosphate (NH3CH2CH2NH2)5Na [Ti2Mo12O30(PO4)(HPO4)4(H2PO4)3]⋅6H2O
T2 - Journal of Chemical Crystallography
AU - Xu, Lin
AU - Sun, Yaqiu
AU - WANG, ENBO
AU - Li, Mingqiang
AU - Hu, Changwen
AU - Huang, Rudan
PY - 2000
DA - 2000/01/01
PB - Springer Nature
SP - 721-726
IS - 11
VL - 30
SN - 1074-1542
SN - 1572-8854
ER -
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@article{2000_Xu,
author = {Lin Xu and Yaqiu Sun and ENBO WANG and Mingqiang Li and Changwen Hu and Rudan Huang},
title = {Hydrothermal synthesis and X-ray structure: A reduced titanic molybdenum(V) phosphate (NH3CH2CH2NH2)5Na [Ti2Mo12O30(PO4)(HPO4)4(H2PO4)3]⋅6H2O},
journal = {Journal of Chemical Crystallography},
year = {2000},
volume = {30},
publisher = {Springer Nature},
month = {jan},
url = {https://doi.org/10.1023/a:1012298127786},
number = {11},
pages = {721--726},
doi = {10.1023/a:1012298127786}
}
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Xu, Lin, et al. “Hydrothermal synthesis and X-ray structure: A reduced titanic molybdenum(V) phosphate (NH3CH2CH2NH2)5Na [Ti2Mo12O30(PO4)(HPO4)4(H2PO4)3]⋅6H2O.” Journal of Chemical Crystallography, vol. 30, no. 11, Jan. 2000, pp. 721-726. https://doi.org/10.1023/a:1012298127786.