Peculiar features of reaction of 2-tert-butoxy-5,6-benzo-1,3,2-dioxaphosphinin-4-one with chloral. Steric structure of 2-chloro-3-trichloromethyl-6,7-benzo-1,4,2λ 5-dioxaphopshepin-5-one 2-oxide
I. V. Konovalova
1, 2
,
L. M. Burnaeva
1, 2
,
V F Mironov
1, 2
,
A.T. Gubaidullin
1, 2
,
A B Dobrynin
1, 2
,
I A Litvinov
1, 2
,
S.V. Romanov
1, 2
,
T A Zyablikova
1, 2
,
O V Yashagina
1, 2
Publication type: Journal Article
Publication date: 2002-01-01
scimago Q4
wos Q4
SJR: 0.179
CiteScore: 1.4
Impact factor: 0.8
ISSN: 10703632, 16083350
General Chemistry
Abstract
The reaction of 2-tert-butoxy-5,6-benzo-1,3,2-dioxaphosphinin-4-one with chloral involves expansion of the six-membered heteroring to form 2-hydroxy-3-trichloromethyl-6,7-benzo-1,4,2λ5-dioxaphosphepin-5-one 2-oxide as a single diastereomer. The product was chlorinated with thionyl chloride to obtain (RS,SR)-2-chloro-3-trichloromethyl-6,7-benzo-1,4,2λ5-dioxaphosphepin-5-one 2-oxide.
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Konovalova I. V. et al. Peculiar features of reaction of 2-tert-butoxy-5,6-benzo-1,3,2-dioxaphosphinin-4-one with chloral. Steric structure of 2-chloro-3-trichloromethyl-6,7-benzo-1,4,2λ 5-dioxaphopshepin-5-one 2-oxide // Russian Journal of General Chemistry. 2002. Vol. 72. No. 8. pp. 1186-1194.
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Konovalova I. V., Burnaeva L. M., Mironov V. F., Gubaidullin A., Dobrynin A. B., Litvinov I. A., Romanov S., Zyablikova T. A., Yashagina O. V. Peculiar features of reaction of 2-tert-butoxy-5,6-benzo-1,3,2-dioxaphosphinin-4-one with chloral. Steric structure of 2-chloro-3-trichloromethyl-6,7-benzo-1,4,2λ 5-dioxaphopshepin-5-one 2-oxide // Russian Journal of General Chemistry. 2002. Vol. 72. No. 8. pp. 1186-1194.
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RIS
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TY - JOUR
DO - 10.1023/A:1020859225163
UR - https://doi.org/10.1023/A:1020859225163
TI - Peculiar features of reaction of 2-tert-butoxy-5,6-benzo-1,3,2-dioxaphosphinin-4-one with chloral. Steric structure of 2-chloro-3-trichloromethyl-6,7-benzo-1,4,2λ 5-dioxaphopshepin-5-one 2-oxide
T2 - Russian Journal of General Chemistry
AU - Konovalova, I. V.
AU - Burnaeva, L. M.
AU - Mironov, V F
AU - Gubaidullin, A.T.
AU - Dobrynin, A B
AU - Litvinov, I A
AU - Romanov, S.V.
AU - Zyablikova, T A
AU - Yashagina, O V
PY - 2002
DA - 2002/01/01
PB - Pleiades Publishing
SP - 1186-1194
IS - 8
VL - 72
SN - 1070-3632
SN - 1608-3350
ER -
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@article{2002_Konovalova,
author = {I. V. Konovalova and L. M. Burnaeva and V F Mironov and A.T. Gubaidullin and A B Dobrynin and I A Litvinov and S.V. Romanov and T A Zyablikova and O V Yashagina},
title = {Peculiar features of reaction of 2-tert-butoxy-5,6-benzo-1,3,2-dioxaphosphinin-4-one with chloral. Steric structure of 2-chloro-3-trichloromethyl-6,7-benzo-1,4,2λ 5-dioxaphopshepin-5-one 2-oxide},
journal = {Russian Journal of General Chemistry},
year = {2002},
volume = {72},
publisher = {Pleiades Publishing},
month = {jan},
url = {https://doi.org/10.1023/A:1020859225163},
number = {8},
pages = {1186--1194},
doi = {10.1023/A:1020859225163}
}
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MLA
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Konovalova, I. V., et al. “Peculiar features of reaction of 2-tert-butoxy-5,6-benzo-1,3,2-dioxaphosphinin-4-one with chloral. Steric structure of 2-chloro-3-trichloromethyl-6,7-benzo-1,4,2λ 5-dioxaphopshepin-5-one 2-oxide.” Russian Journal of General Chemistry, vol. 72, no. 8, Jan. 2002, pp. 1186-1194. https://doi.org/10.1023/A:1020859225163.