Royal Society of Chemistry (RSC)
Dalton Transactions
,  том 51 ,  издание 10 ,  страницы 4113-4121

Cycloaddition of isoselenocyanates to sodium and magnesium metallacycles

Тип публикации: Journal Article
Дата публикации: 2022-02-15
Royal Society of Chemistry (RSC)
scimago Q2
wos Q1
БС1
SJR: 0.653
CiteScore: 6
Impact factor: 3.3
ISSN: 14779226, 14779234
Inorganic Chemistry
Краткое описание
Heterocumulenes SeCNR (R = C6H4OMe-2, C6H4Me-2) undergo facile cycloaddition to [(H-dpp-bian)Na(Et2O)2] (1) (H-dpp-bian = N-protonated 1,2-bis[(2,6-diisopropylphenyl)imino]acenaphthene) resulting in cycloadducts [(H-dpp-bian)Na(SeCNR)(DME)] (2, 3), which are the first cycloadducts derived from a sodium metallacycle reported so far. A comparative reaction of [(dpp-bian)Mg(THF)3] (10) with SeCNR gives magnesium cycloadducts [(dpp-bian)Mg(SeCNR)(Solv)2] (11, 12), which undergo fast decomposition at room temperature. New compounds are characterized by NMR, EPR, and IR spectroscopy, and elemental and X-ray diffraction analysis. Their electronic structures and reaction pathways were probed using DFT calculations.
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Dodonov V. A. et al. Cycloaddition of isoselenocyanates to sodium and magnesium metallacycles // Dalton Transactions. 2022. Vol. 51. No. 10. pp. 4113-4121.
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Dodonov V. A., Kushnerova O. A., Rumyantcev R. V., Novikov A. S., Osmanov V. K., Fedushkin I. L. Cycloaddition of isoselenocyanates to sodium and magnesium metallacycles // Dalton Transactions. 2022. Vol. 51. No. 10. pp. 4113-4121.
RIS |
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TY - JOUR
DO - 10.1039/d1dt04366h
UR - https://xlink.rsc.org/?DOI=D1DT04366H
TI - Cycloaddition of isoselenocyanates to sodium and magnesium metallacycles
T2 - Dalton Transactions
AU - Dodonov, Vladimir A
AU - Kushnerova, Olga A
AU - Rumyantcev, Roman V.
AU - Novikov, Alexander S.
AU - Osmanov, Vladimir K.
AU - Fedushkin, I. L.
PY - 2022
DA - 2022/02/15
PB - Royal Society of Chemistry (RSC)
SP - 4113-4121
IS - 10
VL - 51
PMID - 35187552
SN - 1477-9226
SN - 1477-9234
ER -
BibTex |
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@article{2022_Dodonov,
author = {Vladimir A Dodonov and Olga A Kushnerova and Roman V. Rumyantcev and Alexander S. Novikov and Vladimir K. Osmanov and I. L. Fedushkin},
title = {Cycloaddition of isoselenocyanates to sodium and magnesium metallacycles},
journal = {Dalton Transactions},
year = {2022},
volume = {51},
publisher = {Royal Society of Chemistry (RSC)},
month = {feb},
url = {https://xlink.rsc.org/?DOI=D1DT04366H},
number = {10},
pages = {4113--4121},
doi = {10.1039/d1dt04366h}
}
MLA
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Dodonov, Vladimir A., et al. “Cycloaddition of isoselenocyanates to sodium and magnesium metallacycles.” Dalton Transactions, vol. 51, no. 10, Feb. 2022, pp. 4113-4121. https://xlink.rsc.org/?DOI=D1DT04366H.