A new method for separating the D3and C2visomers of C78
Тип публикации: Journal Article
Дата публикации: 2009-01-01
scimago Q2
wos Q3
БС1
SJR: 0.493
CiteScore: 5
Impact factor: 2.5
ISSN: 11440546, 13699261
Materials Chemistry
General Chemistry
Catalysis
Краткое описание
A new chemical method has been applied to isolate isomers of C78. The photochemical cycloaddition of a mixture of C78(D3) and C78(C2v) with a disilirane affords only the mono-adduct of the C2v isomer of C78. Its counterpart does not give the mono-adduct with a disilirane. The D3 isomer itself and the adduct of the C2v isomer of C78 with a disilirane are easily separated by a HPLC procedure. A facile oxidative desilylation of the adduct takes place, resulting in the formation of pristine C78(C2v). In this context, the separation and isolation of the two isomers of C78 were successfully accomplished by using a silylation–oxidative desilylation process.
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Han A. H. et al. A new method for separating the D3and C2visomers of C78 // New Journal of Chemistry. 2009. Vol. 33. No. 3. pp. 497-500.
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Han A. H., Wakahara T., Maeda Y., Akasaka T., Fujitska M., Ito O., Yamamoto K., Kako M., Kobayashi K., Nagase S. A new method for separating the D3and C2visomers of C78 // New Journal of Chemistry. 2009. Vol. 33. No. 3. pp. 497-500.
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TY - JOUR
DO - 10.1039/b808119k
UR - https://doi.org/10.1039/b808119k
TI - A new method for separating the D3and C2visomers of C78
T2 - New Journal of Chemistry
AU - Han, Ai Hong
AU - Wakahara, Takatsugu
AU - Maeda, Yutaka
AU - Akasaka, Takeshi
AU - Fujitska, Mamoru
AU - Ito, Osamu
AU - Yamamoto, Kazunori
AU - Kako, Masahiro
AU - Kobayashi, Kaoru
AU - Nagase, Shigeru
PY - 2009
DA - 2009/01/01
PB - Royal Society of Chemistry (RSC)
SP - 497-500
IS - 3
VL - 33
SN - 1144-0546
SN - 1369-9261
ER -
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@article{2009_Han,
author = {Ai Hong Han and Takatsugu Wakahara and Yutaka Maeda and Takeshi Akasaka and Mamoru Fujitska and Osamu Ito and Kazunori Yamamoto and Masahiro Kako and Kaoru Kobayashi and Shigeru Nagase},
title = {A new method for separating the D3and C2visomers of C78},
journal = {New Journal of Chemistry},
year = {2009},
volume = {33},
publisher = {Royal Society of Chemistry (RSC)},
month = {jan},
url = {https://doi.org/10.1039/b808119k},
number = {3},
pages = {497--500},
doi = {10.1039/b808119k}
}
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Han, Ai Hong, et al. “A new method for separating the D3and C2visomers of C78.” New Journal of Chemistry, vol. 33, no. 3, Jan. 2009, pp. 497-500. https://doi.org/10.1039/b808119k.