Magnetite nanoparticles coated with ruthenium via SePh layer as a magnetically retrievable catalyst for the selective synthesis of primary amides in an aqueous medium.
Publication type: Journal Article
Publication date: 2014-07-03
scimago Q2
wos Q1
SJR: 0.653
CiteScore: 6.0
Impact factor: 3.3
ISSN: 14779226, 14779234
PubMed ID:
24989230
Inorganic Chemistry
Abstract
The nanostructured magnetic oxide Fe3O4 has been coated with silica and then reacted with phenylselenyl chloride under a N2 atmosphere and RuCl3·xH2O successively in an aqueous medium to prepare Fe3O4@SiO2@SePh@Ru(OH)x nanoparticles (NPs) for the first time. These magnetically retrievable NPs have been authenticated using TEM, SEM-EDX and powder-XRD and found to be an efficient catalyst for one pot conversion (organic solvent not required) of aldehydes, nitriles and benzyl amine to primary amides in water. For aldehydes and nitriles, the yields of primary amides are up to 93%. These NPs can be recycled more than 7 times for the conversion of benzonitrile to the corresponding amide. Gram-scale transformation carried out by using Fe3O4@SiO2@SePh@Ru(OH)x NPs as a catalyst gives ∼86% yield.
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31
Total citations:
31
Citations from 2024:
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(12%)
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GOST
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Joshi H. N. et al. Magnetite nanoparticles coated with ruthenium via SePh layer as a magnetically retrievable catalyst for the selective synthesis of primary amides in an aqueous medium. // Dalton Transactions. 2014. Vol. 43. No. 32. p. 12365.
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Joshi H. N., Sharma K., Sharma A. K., Prakash O., Kumar A., Singh A. Magnetite nanoparticles coated with ruthenium via SePh layer as a magnetically retrievable catalyst for the selective synthesis of primary amides in an aqueous medium. // Dalton Transactions. 2014. Vol. 43. No. 32. p. 12365.
Cite this
RIS
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TY - JOUR
DO - 10.1039/C4DT01189A
UR - https://doi.org/10.1039/C4DT01189A
TI - Magnetite nanoparticles coated with ruthenium via SePh layer as a magnetically retrievable catalyst for the selective synthesis of primary amides in an aqueous medium.
T2 - Dalton Transactions
AU - Joshi, Hemant N.
AU - Sharma, Kamal
AU - Sharma, Alpesh Kumar
AU - Prakash, Om
AU - Kumar, Arvind
AU - Singh, Ajai
PY - 2014
DA - 2014/07/03
PB - Royal Society of Chemistry (RSC)
SP - 12365
IS - 32
VL - 43
PMID - 24989230
SN - 1477-9226
SN - 1477-9234
ER -
Cite this
BibTex (up to 50 authors)
Copy
@article{2014_Joshi,
author = {Hemant N. Joshi and Kamal Sharma and Alpesh Kumar Sharma and Om Prakash and Arvind Kumar and Ajai Singh},
title = {Magnetite nanoparticles coated with ruthenium via SePh layer as a magnetically retrievable catalyst for the selective synthesis of primary amides in an aqueous medium.},
journal = {Dalton Transactions},
year = {2014},
volume = {43},
publisher = {Royal Society of Chemistry (RSC)},
month = {jul},
url = {https://doi.org/10.1039/C4DT01189A},
number = {32},
pages = {12365},
doi = {10.1039/C4DT01189A}
}
Cite this
MLA
Copy
Joshi, Hemant N., et al. “Magnetite nanoparticles coated with ruthenium via SePh layer as a magnetically retrievable catalyst for the selective synthesis of primary amides in an aqueous medium..” Dalton Transactions, vol. 43, no. 32, Jul. 2014, p. 12365. https://doi.org/10.1039/C4DT01189A.
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