Mechanochemical routes for the synthesis of acetyl- and bis-(imino)pyridine ligands and organometallics
Thomas E Shaw
1
,
Lorianne R Shultz
1
,
Louiza R Garayeva
1
,
R. G. Blair
2
,
Bruce C. Noll
3
,
Titel Jurca
1
3
Bruker AXS Inc., 5465 East Cheryl Parkway, Madison, WI, USA
|
Publication type: Journal Article
Publication date: 2018-10-15
scimago Q2
wos Q1
SJR: 0.653
CiteScore: 6.0
Impact factor: 3.3
ISSN: 14779226, 14779234
PubMed ID:
30351333
Inorganic Chemistry
Abstract
Organometallic precatalysts play a pivotal role in organic synthesis. However, their preparation often relies on multiple time, energy, and solvent intensive steps, including the synthesis of supporting organic ligand structures, and finally installation on the desired metal centres. We report the sustainable mechanochemical synthesis of acetyl- and bis-(imino)pyridine pincer complexes, a ubiquitous ligand class for organometallic precatalysts. The approach is extended to the one-pot synthesis of acetyl(imino)pyridine-CoCl2, where the ligand is formed in situ.
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Metrics
17
Total citations:
17
Citations from 2025:
4
(23.53%)
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MLA
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GOST
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Shaw T. E. et al. Mechanochemical routes for the synthesis of acetyl- and bis-(imino)pyridine ligands and organometallics // Dalton Transactions. 2018. Vol. 47. No. 47. pp. 16876-16884.
GOST all authors (up to 50)
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Shaw T. E., Shultz L. R., Garayeva L. R., Blair R. G., Noll B. C., Jurca T. Mechanochemical routes for the synthesis of acetyl- and bis-(imino)pyridine ligands and organometallics // Dalton Transactions. 2018. Vol. 47. No. 47. pp. 16876-16884.
Cite this
RIS
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TY - JOUR
DO - 10.1039/C8DT03608J
UR - https://doi.org/10.1039/C8DT03608J
TI - Mechanochemical routes for the synthesis of acetyl- and bis-(imino)pyridine ligands and organometallics
T2 - Dalton Transactions
AU - Shaw, Thomas E
AU - Shultz, Lorianne R
AU - Garayeva, Louiza R
AU - Blair, R. G.
AU - Noll, Bruce C.
AU - Jurca, Titel
PY - 2018
DA - 2018/10/15
PB - Royal Society of Chemistry (RSC)
SP - 16876-16884
IS - 47
VL - 47
PMID - 30351333
SN - 1477-9226
SN - 1477-9234
ER -
Cite this
BibTex (up to 50 authors)
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@article{2018_Shaw,
author = {Thomas E Shaw and Lorianne R Shultz and Louiza R Garayeva and R. G. Blair and Bruce C. Noll and Titel Jurca},
title = {Mechanochemical routes for the synthesis of acetyl- and bis-(imino)pyridine ligands and organometallics},
journal = {Dalton Transactions},
year = {2018},
volume = {47},
publisher = {Royal Society of Chemistry (RSC)},
month = {oct},
url = {https://doi.org/10.1039/C8DT03608J},
number = {47},
pages = {16876--16884},
doi = {10.1039/C8DT03608J}
}
Cite this
MLA
Copy
Shaw, Thomas E., et al. “Mechanochemical routes for the synthesis of acetyl- and bis-(imino)pyridine ligands and organometallics.” Dalton Transactions, vol. 47, no. 47, Oct. 2018, pp. 16876-16884. https://doi.org/10.1039/C8DT03608J.