Homoleptic trimethylsilylchalcogenolato zincates [Zn(ESiMe3)3]− and stannanides [Sn(ESiMe3)3]− (E = S, Se): precursors in solution-based low-temperature binary metal chalcogenide and Cu2ZnSnS4 (CZTS) synthesis
Тип публикации: Journal Article
Дата публикации: 2020-01-30
scimago Q2
wos Q1
БС1
SJR: 0.653
CiteScore: 6
Impact factor: 3.3
ISSN: 14779226, 14779234
PubMed ID:
32022066
Inorganic Chemistry
Краткое описание
Organic cation salts with homoleptic zincate and stannanide anions, Ph4P [Zn(ESiMe3)3] (E = S (1a), Se (1b)) and Cat [Sn(ESiMe3)3] (Cat = Ph4P+ (E = S (2a-Ph4P); Cat = PPN+ (E = S 2a-Ph4P, Se (2a)) are presented and structurally characterized. Efforts to isolate neutral thermally metastable stannane precursors [Sn(ESiMe3)4] (E = S (3), Se(4)) are reported as well. The thermal decomposition of the presented precursors to yield binary sulfides and selenides of zinc and tin is investigated. Furthermore, the potential of using the title anions as precursors in solution-based low-temperature synthesis of Cu2ZnSnS4 (CZTS) by coprecipitation with [Cu(tmtu)3]PF6 and subsequent annealing is discussed.
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Guschlbauer J. et al. Homoleptic trimethylsilylchalcogenolato zincates [Zn(ESiMe3)3]− and stannanides [Sn(ESiMe3)3]− (E = S, Se): precursors in solution-based low-temperature binary metal chalcogenide and Cu2ZnSnS4 (CZTS) synthesis // Dalton Transactions. 2020. Vol. 49. No. 8. pp. 2517-2526.
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Guschlbauer J., Vollgraff T., Sundermeyer J. Homoleptic trimethylsilylchalcogenolato zincates [Zn(ESiMe3)3]− and stannanides [Sn(ESiMe3)3]− (E = S, Se): precursors in solution-based low-temperature binary metal chalcogenide and Cu2ZnSnS4 (CZTS) synthesis // Dalton Transactions. 2020. Vol. 49. No. 8. pp. 2517-2526.
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TY - JOUR
DO - 10.1039/c9dt04144c
UR - https://xlink.rsc.org/?DOI=C9DT04144C
TI - Homoleptic trimethylsilylchalcogenolato zincates [Zn(ESiMe3)3]− and stannanides [Sn(ESiMe3)3]− (E = S, Se): precursors in solution-based low-temperature binary metal chalcogenide and Cu2ZnSnS4 (CZTS) synthesis
T2 - Dalton Transactions
AU - Guschlbauer, Jannick
AU - Vollgraff, Tobias
AU - Sundermeyer, Jörg
PY - 2020
DA - 2020/01/30
PB - Royal Society of Chemistry (RSC)
SP - 2517-2526
IS - 8
VL - 49
PMID - 32022066
SN - 1477-9226
SN - 1477-9234
ER -
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@article{2020_Guschlbauer,
author = {Jannick Guschlbauer and Tobias Vollgraff and Jörg Sundermeyer},
title = {Homoleptic trimethylsilylchalcogenolato zincates [Zn(ESiMe3)3]− and stannanides [Sn(ESiMe3)3]− (E = S, Se): precursors in solution-based low-temperature binary metal chalcogenide and Cu2ZnSnS4 (CZTS) synthesis},
journal = {Dalton Transactions},
year = {2020},
volume = {49},
publisher = {Royal Society of Chemistry (RSC)},
month = {jan},
url = {https://xlink.rsc.org/?DOI=C9DT04144C},
number = {8},
pages = {2517--2526},
doi = {10.1039/c9dt04144c}
}
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Guschlbauer, Jannick, et al. “Homoleptic trimethylsilylchalcogenolato zincates [Zn(ESiMe3)3]− and stannanides [Sn(ESiMe3)3]− (E = S, Se): precursors in solution-based low-temperature binary metal chalcogenide and Cu2ZnSnS4 (CZTS) synthesis.” Dalton Transactions, vol. 49, no. 8, Jan. 2020, pp. 2517-2526. https://xlink.rsc.org/?DOI=C9DT04144C.