volume 17 issue 30 pages 7131-7134

N-Thiocyanato-dibenzenesulfonimide: a new electrophilic thiocyanating reagent with enhanced reactivity.

Chengqiu LI 1, 2, 3, 4, 5
Pingliang Long 1, 2, 3, 4, 5
Haopeng Wu 1
Hongquan Yin 1
Fuxue Chen 1, 2, 3, 4, 5
Publication typeJournal Article
Publication date2019-07-05
scimago Q2
wos Q2
SJR0.600
CiteScore5.2
Impact factor2.7
ISSN14770520, 14770539
PubMed ID:  31309967
Organic Chemistry
Biochemistry
Physical and Theoretical Chemistry
Abstract
A novel electrophilic thiocyanating reagent, N-thiocyanato-dibenzenesulfonimide, was prepared and exhibited enhanced electrophilicity with a wide scope of substrates. Thus, it reacted with activated aromatics such as phenols, indoles, anilines and anisoles without a catalyst giving the corresponding thicyanate derivatives in high yields, while TfOH for unactivated arenes and hetero aromatics and Zn(OTf)2 for ketones was used as the catalyst, respectively. It is noteworthy that internal alkenes and styrenes were bifunctionalized giving 1,2-amino thiocyanates in high yields.
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GOST |
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GOST Copy
LI C. et al. N-Thiocyanato-dibenzenesulfonimide: a new electrophilic thiocyanating reagent with enhanced reactivity. // Organic and Biomolecular Chemistry. 2019. Vol. 17. No. 30. pp. 7131-7134.
GOST all authors (up to 50) Copy
LI C., Long P., Wu H., Yin H., Chen F. N-Thiocyanato-dibenzenesulfonimide: a new electrophilic thiocyanating reagent with enhanced reactivity. // Organic and Biomolecular Chemistry. 2019. Vol. 17. No. 30. pp. 7131-7134.
RIS |
Cite this
RIS Copy
TY - JOUR
DO - 10.1039/C9OB01340G
UR - https://xlink.rsc.org/?DOI=C9OB01340G
TI - N-Thiocyanato-dibenzenesulfonimide: a new electrophilic thiocyanating reagent with enhanced reactivity.
T2 - Organic and Biomolecular Chemistry
AU - LI, Chengqiu
AU - Long, Pingliang
AU - Wu, Haopeng
AU - Yin, Hongquan
AU - Chen, Fuxue
PY - 2019
DA - 2019/07/05
PB - Royal Society of Chemistry (RSC)
SP - 7131-7134
IS - 30
VL - 17
PMID - 31309967
SN - 1477-0520
SN - 1477-0539
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2019_LI,
author = {Chengqiu LI and Pingliang Long and Haopeng Wu and Hongquan Yin and Fuxue Chen},
title = {N-Thiocyanato-dibenzenesulfonimide: a new electrophilic thiocyanating reagent with enhanced reactivity.},
journal = {Organic and Biomolecular Chemistry},
year = {2019},
volume = {17},
publisher = {Royal Society of Chemistry (RSC)},
month = {jul},
url = {https://xlink.rsc.org/?DOI=C9OB01340G},
number = {30},
pages = {7131--7134},
doi = {10.1039/C9OB01340G}
}
MLA
Cite this
MLA Copy
LI, Chengqiu, et al. “N-Thiocyanato-dibenzenesulfonimide: a new electrophilic thiocyanating reagent with enhanced reactivity..” Organic and Biomolecular Chemistry, vol. 17, no. 30, Jul. 2019, pp. 7131-7134. https://xlink.rsc.org/?DOI=C9OB01340G.