Electroassisted catalysis of the reductive coupling of 2-bromooctane and methyl vinyl ketone by a binuclear cobalt–salen–iron complex in DMF solution: electrosynthesis and cyclic voltammetry analysis
Тип публикации: Journal Article
Дата публикации: 1999-01-01
scimago Q2
wos Q3
БС1
SJR: 0.493
CiteScore: 5
Impact factor: 2.5
ISSN: 11440546, 13699261
Materials Chemistry
General Chemistry
Catalysis
Краткое описание
We report in this study the combined use of a CoSalen [H2Salen=bis(salicylidene)ethane-1,2-diamine] complex and an undivided electrochemical cell process in the electroassisted reductive coupling of 2-bromooctane and methyl vinyl ketone with satisfactory results. Correlation between the electroanalytical analysis of the reactivity of CoSalen in the presence of 2-bromooctane and methyl vinyl ketone and the electrosynthesis performed in an undivided electrochemical cell with a sacrificial iron anode allows us to suggest that a heterobinuclear Co–Salen–Fe complex is the effective catalyst of the considered reaction. Stability of this intermediate during preparative electrolysis is also discussed.
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Cannes C. et al. Electroassisted catalysis of the reductive coupling of 2-bromooctane and methyl vinyl ketone by a binuclear cobalt–salen–iron complex in DMF solution: electrosynthesis and cyclic voltammetry analysis // New Journal of Chemistry. 1999. Vol. 23. No. 5. pp. 489-494.
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Cannes C., Bedioui F., Condon-Gueugnot S., Yves Nedelec J., Devynck J. Electroassisted catalysis of the reductive coupling of 2-bromooctane and methyl vinyl ketone by a binuclear cobalt–salen–iron complex in DMF solution: electrosynthesis and cyclic voltammetry analysis // New Journal of Chemistry. 1999. Vol. 23. No. 5. pp. 489-494.
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TY - JOUR
DO - 10.1039/a900274j
UR - https://doi.org/10.1039/a900274j
TI - Electroassisted catalysis of the reductive coupling of 2-bromooctane and methyl vinyl ketone by a binuclear cobalt–salen–iron complex in DMF solution: electrosynthesis and cyclic voltammetry analysis
T2 - New Journal of Chemistry
AU - Cannes, Celine
AU - Bedioui, Fethi
AU - Condon-Gueugnot, Sylvie
AU - Yves Nedelec, Jean
AU - Devynck, Jacques
PY - 1999
DA - 1999/01/01
PB - Royal Society of Chemistry (RSC)
SP - 489-494
IS - 5
VL - 23
SN - 1144-0546
SN - 1369-9261
ER -
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@article{1999_Cannes,
author = {Celine Cannes and Fethi Bedioui and Sylvie Condon-Gueugnot and Jean Yves Nedelec and Jacques Devynck},
title = {Electroassisted catalysis of the reductive coupling of 2-bromooctane and methyl vinyl ketone by a binuclear cobalt–salen–iron complex in DMF solution: electrosynthesis and cyclic voltammetry analysis},
journal = {New Journal of Chemistry},
year = {1999},
volume = {23},
publisher = {Royal Society of Chemistry (RSC)},
month = {jan},
url = {https://doi.org/10.1039/a900274j},
number = {5},
pages = {489--494},
doi = {10.1039/a900274j}
}
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Cannes, Celine, et al. “Electroassisted catalysis of the reductive coupling of 2-bromooctane and methyl vinyl ketone by a binuclear cobalt–salen–iron complex in DMF solution: electrosynthesis and cyclic voltammetry analysis.” New Journal of Chemistry, vol. 23, no. 5, Jan. 1999, pp. 489-494. https://doi.org/10.1039/a900274j.