(Fluoren-9-ylmethoxy)carbonyl (Fmoc) amino acid azides: Synthesis, isolation, characterisation, stability and application to synthesis of peptides
Тип публикации: Journal Article
Дата публикации: 2000-01-01
SJR: 1.151
CiteScore: —
Impact factor: —
ISSN: 0300922X, 13645463, 14727781
General Medicine
Краткое описание
The synthesis of Fmoc amino acid azides starting from the corresponding protected amino acid and sodium azide (NaN3) by the mixed anhydride method using isobutoxycarbonyl chloride (IBC-Cl) or by the acid chloride method is described. Isolated as crystalline solids, they are stable at room temperature, with a long shelf-life, as well as in aqueous washing operations. They are useful as coupling agents in peptide synthesis.
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ГОСТ
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Babu V. V. S., Ananda K., Vasanthakumar G. (Fluoren-9-ylmethoxy)carbonyl (Fmoc) amino acid azides: Synthesis, isolation, characterisation, stability and application to synthesis of peptides // Journal of the Chemical Society Perkin Transactions 1. 2000. Vol. 24. pp. 4328-4331.
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Babu V. V. S., Ananda K., Vasanthakumar G. (Fluoren-9-ylmethoxy)carbonyl (Fmoc) amino acid azides: Synthesis, isolation, characterisation, stability and application to synthesis of peptides // Journal of the Chemical Society Perkin Transactions 1. 2000. Vol. 24. pp. 4328-4331.
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TY - JOUR
DO - 10.1039/b006756n
UR - https://doi.org/10.1039/b006756n
TI - (Fluoren-9-ylmethoxy)carbonyl (Fmoc) amino acid azides: Synthesis, isolation, characterisation, stability and application to synthesis of peptides
T2 - Journal of the Chemical Society Perkin Transactions 1
AU - Babu, Vommina V. Suresh
AU - Ananda, Kuppanna
AU - Vasanthakumar, Ganga-Ramu
PY - 2000
DA - 2000/01/01
PB - Royal Society of Chemistry (RSC)
SP - 4328-4331
IS - 24
SN - 0300-922X
SN - 1364-5463
SN - 1472-7781
ER -
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BibTex (до 50 авторов)
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@article{2000_Babu,
author = {Vommina V. Suresh Babu and Kuppanna Ananda and Ganga-Ramu Vasanthakumar},
title = {(Fluoren-9-ylmethoxy)carbonyl (Fmoc) amino acid azides: Synthesis, isolation, characterisation, stability and application to synthesis of peptides},
journal = {Journal of the Chemical Society Perkin Transactions 1},
year = {2000},
publisher = {Royal Society of Chemistry (RSC)},
month = {jan},
url = {https://doi.org/10.1039/b006756n},
number = {24},
pages = {4328--4331},
doi = {10.1039/b006756n}
}
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