ansa-metallocenes with a Ph2 Si bridge: Molecular structures of HfCl2 [Ph2 Si(η5-C13 H8 )(η5-C5 H4 )] and HfCl2 [Ph2 Si(C13 H9 ) (η5-C5 H4 )]2
Тип публикации: Journal Article
Дата публикации: 2001-01-01
SJR: —
CiteScore: —
Impact factor: —
ISSN: 14727773, 13645447, 1470479X, 03009246
General Chemistry
Краткое описание
A mixture of rac- and meso-HfCl2[Ph2Si(η5-C9H6)2] was synthesized by treatment of HfCl4 with the dilithium salt of di(1H-inden-1-yl)diphenylsilane. These complexes were isolated after fractional crystallization in 15.5 and 8.5% yields, respectively. A sterically strained ansa complex HfCl2[Ph2Si(η5-C13H8)(η5-C5H4)] was synthesized in 62% yield by treatment of HfCl4 with the dilithium salt of cyclopentadienyl(fluoren-9-yl)diphenylsilane. Both this compound, and the by-product of reaction, HfCl2[Ph2Si(C13H9)(η5-C5H4)]2, were characterized by crystal structure analysis.
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Izmer V. V. et al. ansa-metallocenes with a Ph2Si bridge: Molecular structures of HfCl2[Ph2Si(η5-C13 H8)(η5-C5H4)] and HfCl2[Ph2Si(C13H9) (η5-C5H4)]2 // Journal of the Chemical Society Dalton Transactions. 2001. Vol. 7. pp. 1131-1136.
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Izmer V. V., Agarkov A. Y., Nosova V. M., Kuz'mina L. G., Howard J. A., Beletskaya I. P., Voskoboynikov A. Z. ansa-metallocenes with a Ph2Si bridge: Molecular structures of HfCl2[Ph2Si(η5-C13 H8)(η5-C5H4)] and HfCl2[Ph2Si(C13H9) (η5-C5H4)]2 // Journal of the Chemical Society Dalton Transactions. 2001. Vol. 7. pp. 1131-1136.
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TY - JOUR
DO - 10.1039/b009280k
UR - https://doi.org/10.1039/b009280k
TI - ansa-metallocenes with a Ph2Si bridge: Molecular structures of HfCl2[Ph2Si(η5-C13 H8)(η5-C5H4)] and HfCl2[Ph2Si(C13H9) (η5-C5H4)]2
T2 - Journal of the Chemical Society Dalton Transactions
AU - Izmer, Vyacheslav V
AU - Agarkov, Anton Y
AU - Nosova, Valentina M
AU - Kuz'mina, Lyudmila G.
AU - Howard, Judith A.
AU - Beletskaya, Irina P.
AU - Voskoboynikov, Alexander Z.
PY - 2001
DA - 2001/01/01
PB - Royal Society of Chemistry (RSC)
SP - 1131-1136
IS - 7
SN - 1472-7773
SN - 1364-5447
SN - 1470-479X
SN - 0300-9246
ER -
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@article{2001_Izmer,
author = {Vyacheslav V Izmer and Anton Y Agarkov and Valentina M Nosova and Lyudmila G. Kuz'mina and Judith A. Howard and Irina P. Beletskaya and Alexander Z. Voskoboynikov},
title = {ansa-metallocenes with a Ph2Si bridge: Molecular structures of HfCl2[Ph2Si(η5-C13 H8)(η5-C5H4)] and HfCl2[Ph2Si(C13H9) (η5-C5H4)]2},
journal = {Journal of the Chemical Society Dalton Transactions},
year = {2001},
publisher = {Royal Society of Chemistry (RSC)},
month = {jan},
url = {https://doi.org/10.1039/b009280k},
number = {7},
pages = {1131--1136},
doi = {10.1039/b009280k}
}
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