issue 18 pages 1774-1775

1,2,4,3,5-Benzotrithiadiazepine and its unexpected hydrolysis to unusual 7H,14H-dibenzo[d,i][1,2,6,7,3,8]tetrathiadiazecine

Publication typeJournal Article
Publication date2001-01-01
scimago Q1
wos Q2
SJR1.037
CiteScore7.4
Impact factor4.2
ISSN13597345, 1364548X
PubMed ID:  12240309
Materials Chemistry
Metals and Alloys
Surfaces, Coatings and Films
General Chemistry
Ceramics and Composites
Electronic, Optical and Magnetic Materials
Catalysis
Abstract
Previously unknown 1,2,4,3,5-benzotrithiadiazepine 1 was prepared by 1:1 condensation of Ph-N=S=N-SiMe3 with S2Cl2 followed by intramolecular ortho-cyclization of [Ph-N=S=N-S-S-Cl] intermediate, and hydrolyzed in pyridine to unusual macrocyclic 7H,14H-dibenzo[d,i][1,2,6,7,3,8]tetrathiadiazecine 2.
Found 

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GOST Copy
Makarov A. et al. 1,2,4,3,5-Benzotrithiadiazepine and its unexpected hydrolysis to unusual 7H,14H-dibenzo[d,i][1,2,6,7,3,8]tetrathiadiazecine // Chemical Communications. 2001. Vol. 18. pp. 1774-1775.
GOST all authors (up to 50) Copy
Makarov A., Shakirov M. M., Bagryanskaya I. Y., Bagryanskaya I. Y., Gatilov Y. V., Zibarev A. V. 1,2,4,3,5-Benzotrithiadiazepine and its unexpected hydrolysis to unusual 7H,14H-dibenzo[d,i][1,2,6,7,3,8]tetrathiadiazecine // Chemical Communications. 2001. Vol. 18. pp. 1774-1775.
RIS |
Cite this
RIS Copy
TY - JOUR
DO - 10.1039/b105001j
UR - https://doi.org/10.1039/b105001j
TI - 1,2,4,3,5-Benzotrithiadiazepine and its unexpected hydrolysis to unusual 7H,14H-dibenzo[d,i][1,2,6,7,3,8]tetrathiadiazecine
T2 - Chemical Communications
AU - Makarov, Alexander
AU - Shakirov, Makhmut M.
AU - Bagryanskaya, Irina Yu.
AU - Bagryanskaya, Irina Yu.
AU - Gatilov, Yuri V.
AU - Zibarev, Andrey V.
PY - 2001
DA - 2001/01/01
PB - Royal Society of Chemistry (RSC)
SP - 1774-1775
IS - 18
PMID - 12240309
SN - 1359-7345
SN - 1364-548X
ER -
BibTex
Cite this
BibTex (up to 50 authors) Copy
@article{2001_Makarov,
author = {Alexander Makarov and Makhmut M. Shakirov and Irina Yu. Bagryanskaya and Irina Yu. Bagryanskaya and Yuri V. Gatilov and Andrey V. Zibarev},
title = {1,2,4,3,5-Benzotrithiadiazepine and its unexpected hydrolysis to unusual 7H,14H-dibenzo[d,i][1,2,6,7,3,8]tetrathiadiazecine},
journal = {Chemical Communications},
year = {2001},
publisher = {Royal Society of Chemistry (RSC)},
month = {jan},
url = {https://doi.org/10.1039/b105001j},
number = {18},
pages = {1774--1775},
doi = {10.1039/b105001j}
}