Journal of Materials Chemistry A

, volume 22 , issue 48 , pages 25123

The poly(ethylene glycol) assisted preparation of NH4TiOF3 mesocrystals and their topotactic conversion to TiO2

Masashi Inoguchi ^{1, 2}

Mohammad Afzaal ^{2, 3}

Nobuhiko TANAKA ¹

Peter O’Brien ²

Hide authors affiliations Show authors affiliations: 3 affiliations

Murata Manufacturing Co., Ltd., Nagaokakyo-shi, Kyoto 617-8555, Japan |

The Manchester Materials Science Centre and The School of Chemistry, The University of Manchester, Oxford Road, Manchester, UK |

Center of Research Excellence in Renewable Energy, King Fahd University of Petroleum and Minerals, PO Box 1292, Dhahran, Saudi Arabia |

Publication type: Journal Article

Publication date: 2012-10-18

Royal Society of Chemistry (RSC)

Journal of Materials Chemistry A

scimago Q1

wos Q1

SJR: 2.462

CiteScore: 16.7

Impact factor: 9.5

ISSN: 20507488, 20507496, 09599428, 13645501

DOI: 10.1039/c2jm30872j

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Materials Chemistry

General Chemistry

Abstract

Poly(ethylene glycols) with different molecular weights were used to prepare NH4TiOF3 mesocrystals. The use of PEG-1000, -10 000, or -20 000 produced NH4TiOF3 mesocrystals whereas, PEG-4500 produced TiO2 (anatase) in nanoparticulate form. The shapes and the crystal structures of NH4TiOF3 mesocrystals formed with PEGs are similar to those obtained with the Brij family of nonionic surfactants. The conversion of NH4TiOF3 mesocrystals prepared with PEG-20 000 to TiO2 (anatase) mesocrystals by heat treatment or washing with boric acid was also studied. The TiO2 mesocrystals retained the crystallographical orientation of the parent NH4TiOF3 mesocrystals and the apparent average sizes of the nanoparticles are between several and tens of nanometers.

Found

2 citations

Ivanov Vladimir

🥼

DSc in Chemistry, full member of the Russian Academy of Sciences

513 publications, 6 841 citations, 137 reviews

h-index: 37

Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences

Lomonosov Moscow State University

National Research University Higher School of Economics

Solid state chemistry

1 citation

Baranchikov Alexander

PhD in Chemistry

401 publications, 5 280 citations, 274 reviews

h-index: 32

Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences

Research interests

Hydrothermal synthesis

Inorganic Chemistry

Low-temperature nitrogen adsorption

Rare-earth elements

Scanning electron microscopy

X-ray diffraction (XRD)

1 citation

Naranov Evgeny

🥼 🤝

PhD in Chemistry

53 publications, 676 citations, 14 reviews

h-index: 14

Lomonosov Moscow State University

A.V. Topchiev Institute of Petrochemical Synthesis RAS

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GOST |

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Inoguchi M. et al. The poly(ethylene glycol) assisted preparation of NH4TiOF3 mesocrystals and their topotactic conversion to TiO2 // Journal of Materials Chemistry A. 2012. Vol. 22. No. 48. p. 25123.

GOST all authors (up to 50) Copy

Inoguchi M., Afzaal M., TANAKA N., O’Brien P. The poly(ethylene glycol) assisted preparation of NH4TiOF3 mesocrystals and their topotactic conversion to TiO2 // Journal of Materials Chemistry A. 2012. Vol. 22. No. 48. p. 25123.

RIS |

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RIS Copy

TY - JOUR

DO - 10.1039/c2jm30872j

UR - https://doi.org/10.1039/c2jm30872j

TI - The poly(ethylene glycol) assisted preparation of NH4TiOF3 mesocrystals and their topotactic conversion to TiO2

T2 - Journal of Materials Chemistry A

AU - Inoguchi, Masashi

AU - Afzaal, Mohammad

AU - TANAKA, Nobuhiko

AU - O’Brien, Peter

PY - 2012

DA - 2012/10/18

PB - Royal Society of Chemistry (RSC)

SP - 25123

IS - 48

VL - 22

SN - 2050-7488

SN - 2050-7496

SN - 0959-9428

SN - 1364-5501

ER -

BibTex |

Cite this

BibTex (up to 50 authors) Copy

@article{2012_Inoguchi,

author = {Masashi Inoguchi and Mohammad Afzaal and Nobuhiko TANAKA and Peter O’Brien},

title = {The poly(ethylene glycol) assisted preparation of NH4TiOF3 mesocrystals and their topotactic conversion to TiO2},

journal = {Journal of Materials Chemistry A},

year = {2012},

volume = {22},

publisher = {Royal Society of Chemistry (RSC)},

month = {oct},

url = {https://doi.org/10.1039/c2jm30872j},

number = {48},

pages = {25123},

doi = {10.1039/c2jm30872j}

}

MLA

Cite this

MLA Copy

Inoguchi, Masashi, et al. “The poly(ethylene glycol) assisted preparation of NH4TiOF3 mesocrystals and their topotactic conversion to TiO2.” Journal of Materials Chemistry A, vol. 22, no. 48, Oct. 2012, p. 25123. https://doi.org/10.1039/c2jm30872j.

Publisher

Royal Society of Chemistry (RSC)

Journal

Journal of Materials Chemistry A

scimago Q1

wos Q1

SJR

2.462

CiteScore

16.7

Impact factor

9.5

ISSN

20507488 (Print)

20507496 (Electronic)

09599428 (Print)

13645501 (Electronic)