Hypervalent iodine in organic synthesis. A novel route to the dihydroxyacetone side-chain in the pregnene series
Тип публикации: Journal Article
Дата публикации: 1981-01-01
SJR: —
CiteScore: —
Impact factor: —
ISSN: 00224936
Molecular Medicine
Краткое описание
Treatment of pregnenolone (1) with PhIO and KOH in MeOH yields 3β,21-dihydroxypregn-5-en-20-one dimethyl acetal (2) from which a molecule of MeOH is lost to yield the C(17)–C(20) enol methyl ether (3) which may be epoxidized and hydrolysed to yield the C-17-dihydroxyacetone side-chain in the correct configuration as in 3β,17α,21-trihydroxypregn-5-en-20-one (4).
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Moriarty R. M., John L. S., Du P. C. Hypervalent iodine in organic synthesis. A novel route to the dihydroxyacetone side-chain in the pregnene series // Journal of the Chemical Society Chemical Communications. 1981. Vol. 13. p. 641.
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Moriarty R. M., John L. S., Du P. C. Hypervalent iodine in organic synthesis. A novel route to the dihydroxyacetone side-chain in the pregnene series // Journal of the Chemical Society Chemical Communications. 1981. Vol. 13. p. 641.
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TY - JOUR
DO - 10.1039/c39810000641
UR - https://doi.org/10.1039/c39810000641
TI - Hypervalent iodine in organic synthesis. A novel route to the dihydroxyacetone side-chain in the pregnene series
T2 - Journal of the Chemical Society Chemical Communications
AU - Moriarty, Robert M
AU - John, Lian S
AU - Du, Pin C
PY - 1981
DA - 1981/01/01
PB - Royal Society of Chemistry (RSC)
SP - 641
IS - 13
SN - 0022-4936
ER -
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BibTex (до 50 авторов)
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@article{1981_Moriarty,
author = {Robert M Moriarty and Lian S John and Pin C Du},
title = {Hypervalent iodine in organic synthesis. A novel route to the dihydroxyacetone side-chain in the pregnene series},
journal = {Journal of the Chemical Society Chemical Communications},
year = {1981},
publisher = {Royal Society of Chemistry (RSC)},
month = {jan},
url = {https://doi.org/10.1039/c39810000641},
number = {13},
pages = {641},
doi = {10.1039/c39810000641}
}