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High-resolution solid-state 13C and 29Si NMR investigations of the dynamic properties of tetrakis(trimethylsilyl)silane

Тип публикацииJournal Article
Дата публикации1993-01-01
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ISSN00224936
Molecular Medicine
Краткое описание
High-resolution solid-state 13C and 29Si NMR spectroscopy have been used to investigate the dynamic properties of tetrakis(trimethylsilyl)silane (TTMSS) as a function of temperature; from the temperature dependence of the spectra, it is clear that TTMSS is not useful as a chemical shift reference material below ca. 238K, but the spectral changes associated with the phase transition at this temperature nevertheless provide a precise method for controlling temperature calibration in low-temperature solid-state 13C NMR studies.
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Aliev A. E., Harris K. D., Apperley D. C. High-resolution solid-state 13C and 29Si NMR investigations of the dynamic properties of tetrakis(trimethylsilyl)silane // Journal of the Chemical Society Chemical Communications. 1993. Vol. 3. p. 251.
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Aliev A. E., Harris K. D., Apperley D. C. High-resolution solid-state 13C and 29Si NMR investigations of the dynamic properties of tetrakis(trimethylsilyl)silane // Journal of the Chemical Society Chemical Communications. 1993. Vol. 3. p. 251.
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TY - JOUR
DO - 10.1039/c39930000251
UR - https://doi.org/10.1039/c39930000251
TI - High-resolution solid-state 13C and 29Si NMR investigations of the dynamic properties of tetrakis(trimethylsilyl)silane
T2 - Journal of the Chemical Society Chemical Communications
AU - Aliev, Abil E.
AU - Harris, Kenneth D.
AU - Apperley, David C.
PY - 1993
DA - 1993/01/01
PB - Royal Society of Chemistry (RSC)
SP - 251
IS - 3
SN - 0022-4936
ER -
BibTex
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@article{1993_Aliev,
author = {Abil E. Aliev and Kenneth D. Harris and David C. Apperley},
title = {High-resolution solid-state 13C and 29Si NMR investigations of the dynamic properties of tetrakis(trimethylsilyl)silane},
journal = {Journal of the Chemical Society Chemical Communications},
year = {1993},
publisher = {Royal Society of Chemistry (RSC)},
month = {jan},
url = {https://doi.org/10.1039/c39930000251},
number = {3},
pages = {251},
doi = {10.1039/c39930000251}
}