Physical Chemistry Chemical Physics, volume 18, issue 6, pages 4617-4626
High-temperature X-ray diffraction and thermal expansion of nanocrystalline and coarse-crystalline acanthite α-Ag2S and argentite β-Ag2S
Publication type: Journal Article
Publication date: 2016-01-22
Journal:
Physical Chemistry Chemical Physics
Quartile SCImago
Q1
Quartile WOS
Q2
Impact factor: 3.3
ISSN: 14639076, 14639084
Physical and Theoretical Chemistry
General Physics and Astronomy
Abstract
An in situ study of thermal expansion of polymorphic phases of coarse-crystalline and nanocrystalline silver sulfide - monoclinic acanthite α-Ag2S and cubic argentite β-Ag2S - has been carried out for the first time using the high-temperature X-ray diffraction method. The temperature dependencies of the unit cell parameters of acanthite and argentite in the interval of 300-623 K have been determined, and the thermal expansion coefficients of acanthite and argentite have been found. It is shown that the observed difference in the thermal expansion coefficients for nano- and coarse-crystalline acanthite is due to the small particle size of nanocrystalline silver sulfide leading to the growth of anharmonicity of atomic vibrations. It is established by differential thermal analysis that a reversible polymorphic acanthite-argentite phase transformation takes place at ∼449-450 K and the phase transformation enthalpy is equal to ∼3.7-3.9 kJ mol(-1).
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Citations by publishers
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2 publications, 3.33%
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1 publication, 1.67%
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World Scientific
1 publication, 1.67%
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- We do not take into account publications without a DOI.
- Statistics recalculated only for publications connected to researchers, organizations and labs registered on the platform.
- Statistics recalculated weekly.
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Sadovnikov S. I. et al. High-temperature X-ray diffraction and thermal expansion of nanocrystalline and coarse-crystalline acanthite α-Ag2S and argentite β-Ag2S // Physical Chemistry Chemical Physics. 2016. Vol. 18. No. 6. pp. 4617-4626.
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Sadovnikov S. I., Gusev A. I., Chukin A., Rempel A. High-temperature X-ray diffraction and thermal expansion of nanocrystalline and coarse-crystalline acanthite α-Ag2S and argentite β-Ag2S // Physical Chemistry Chemical Physics. 2016. Vol. 18. No. 6. pp. 4617-4626.
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TY - JOUR
DO - 10.1039/c5cp07224g
UR - https://doi.org/10.1039/c5cp07224g
TI - High-temperature X-ray diffraction and thermal expansion of nanocrystalline and coarse-crystalline acanthite α-Ag2S and argentite β-Ag2S
T2 - Physical Chemistry Chemical Physics
AU - Sadovnikov, Stanislav I
AU - Chukin, A.V.
AU - Gusev, Aleksandr I.
AU - Rempel, Andrey
PY - 2016
DA - 2016/01/22 00:00:00
PB - Royal Society of Chemistry (RSC)
SP - 4617-4626
IS - 6
VL - 18
SN - 1463-9076
SN - 1463-9084
ER -
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@article{2016_Sadovnikov,
author = {Stanislav I Sadovnikov and A.V. Chukin and Aleksandr I. Gusev and Andrey Rempel},
title = {High-temperature X-ray diffraction and thermal expansion of nanocrystalline and coarse-crystalline acanthite α-Ag2S and argentite β-Ag2S},
journal = {Physical Chemistry Chemical Physics},
year = {2016},
volume = {18},
publisher = {Royal Society of Chemistry (RSC)},
month = {jan},
url = {https://doi.org/10.1039/c5cp07224g},
number = {6},
pages = {4617--4626},
doi = {10.1039/c5cp07224g}
}
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MLA
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Sadovnikov, Stanislav I., et al. “High-temperature X-ray diffraction and thermal expansion of nanocrystalline and coarse-crystalline acanthite α-Ag2S and argentite β-Ag2S.” Physical Chemistry Chemical Physics, vol. 18, no. 6, Jan. 2016, pp. 4617-4626. https://doi.org/10.1039/c5cp07224g.
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