CrystEngComm, volume 18, issue 39, pages 7506-7515
Peculiarities of styryl dyes of the benzoselenazole series crystal packings and their influence on solid phase [2 + 2] photocycloaddition reaction with single crystal retention
Publication type: Journal Article
Publication date: 2016-08-22
General Chemistry
Condensed Matter Physics
General Materials Science
Abstract
New styryl dyes of the 2-benzoselenazole series which contain iodide, triiodide, and tosylate anions were synthesized. Crystals of these compounds were grown in different crystal forms – solvent free and hydroquinone, benzene or ethyl acetate solvated ones. X-ray structural studies of the crystals shows that those containing tosylate and triiodide anions form the centrosymmetrically related stacking motif, typical for styryl dye cations and favorable for [2 + 2] photocycloaddition (PCA) reactions. This reaction takes place in crystals with tosylate anions as a single crystal-to-single crystal process. On the contrary, in the triiodide dye crystals, the PCA reaction is lacking, probably due to a weak directional interaction of the selenium atoms with the anions. The iodide dye crystals demonstrate non-typical packing for styryl dyes and manifest as a two-dimensional close packing motif of the cations which is unfavorable for cycloaddition.
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Crystallography Reports
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Inorganica Chimica Acta
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Citations by publishers
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Pleiades Publishing
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Pleiades Publishing
1 publication, 20%
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Elsevier
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Elsevier
1 publication, 20%
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Springer Nature
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Springer Nature
1 publication, 20%
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Royal Society of Chemistry (RSC)
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Royal Society of Chemistry (RSC)
1 publication, 20%
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RTU MIREA
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RTU MIREA
1 publication, 20%
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Kuz'mina L. G. et al. Peculiarities of styryl dyes of the benzoselenazole series crystal packings and their influence on solid phase [2 + 2] photocycloaddition reaction with single crystal retention // CrystEngComm. 2016. Vol. 18. No. 39. pp. 7506-7515.
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Kuz'mina L. G., Vedernikov A. I., Howard J. A., Bezzubov S. I., Alfimov M. V., Fomina M. V. Peculiarities of styryl dyes of the benzoselenazole series crystal packings and their influence on solid phase [2 + 2] photocycloaddition reaction with single crystal retention // CrystEngComm. 2016. Vol. 18. No. 39. pp. 7506-7515.
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TY - JOUR
DO - 10.1039/c6ce01426g
UR - https://doi.org/10.1039%2Fc6ce01426g
TI - Peculiarities of styryl dyes of the benzoselenazole series crystal packings and their influence on solid phase [2 + 2] photocycloaddition reaction with single crystal retention
T2 - CrystEngComm
AU - Kuz'mina, Lyudmila G.
AU - Vedernikov, Artem I.
AU - Alfimov, Michael V
AU - Howard, Judith A.
AU - Bezzubov, Stanislav I.
AU - Fomina, Marina V.
PY - 2016
DA - 2016/08/22 00:00:00
PB - Royal Society of Chemistry (RSC)
SP - 7506-7515
IS - 39
VL - 18
SN - 1466-8033
ER -
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@article{2016_Kuz'mina,
author = {Lyudmila G. Kuz'mina and Artem I. Vedernikov and Michael V Alfimov and Judith A. Howard and Stanislav I. Bezzubov and Marina V. Fomina},
title = {Peculiarities of styryl dyes of the benzoselenazole series crystal packings and their influence on solid phase [2 + 2] photocycloaddition reaction with single crystal retention},
journal = {CrystEngComm},
year = {2016},
volume = {18},
publisher = {Royal Society of Chemistry (RSC)},
month = {aug},
url = {https://doi.org/10.1039%2Fc6ce01426g},
number = {39},
pages = {7506--7515},
doi = {10.1039/c6ce01426g}
}
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Kuz'mina, Lyudmila G., et al. “Peculiarities of styryl dyes of the benzoselenazole series crystal packings and their influence on solid phase [2 + 2] photocycloaddition reaction with single crystal retention.” CrystEngComm, vol. 18, no. 39, Aug. 2016, pp. 7506-7515. https://doi.org/10.1039%2Fc6ce01426g.