Analytical Methods

, том 9 , издание 45 , страницы 6335-6340

A novel trityl/acridine derivatization agent for analysis of thiols by (matrix-assisted)(nanowire-assisted)laser desorption/ionization and electrospray ionization mass spectrometry

Тип публикации: Journal Article

Дата публикации: 2017-10-30

Royal Society of Chemistry (RSC)

Analytical Methods

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SJR: 0.478

CiteScore: 4.5

Impact factor: 2.6

ISSN: 17599660, 17599679

DOI: 10.1039/c7ay01965c

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General Chemical Engineering

Analytical Chemistry

General Engineering

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The derivatization reagent was prepared in situ by the reaction of tris(2,6-dimethoxyphenyl)methylium hexafluorophosphate with N-(2-aminoethyl)maleimide and used for the modification of a number of low molecular weight thiols. The adducts were analyzed by (MA)(NA)LDI MS and ESI MS. All registered mass spectra ((MA)(NA)LDI, ESI) revealed intense peaks of the cations of the derivatization products. The increment of the derivatization agent (499 Da) shifts the ion peaks of analytes from noisy low mass regions, thus allowing the detection of low molecular weight thiols. LDI analysis of the natural-gas condensate sample showed the presence of saturated alkylthiols (up to C22H45SH).

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Топ-30

Журналы

	1
Petroleum Chemistry	Petroleum Chemistry, 1, 20% Petroleum Chemistry 1 публикация, 20%
Journal of Chromatography A	Journal of Chromatography A, 1, 20% Journal of Chromatography A 1 публикация, 20%
Journal of Analytical Chemistry	Journal of Analytical Chemistry, 1, 20% Journal of Analytical Chemistry 1 публикация, 20%
Chromatographia	Chromatographia, 1, 20% Chromatographia 1 публикация, 20%
	1

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Pleiades Publishing	Pleiades Publishing, 2, 40% Pleiades Publishing 2 публикации, 40%
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Wiley	Wiley, 1, 20% Wiley 1 публикация, 20%
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Topolyan A. P. et al. A novel trityl/acridine derivatization agent for analysis of thiols by (matrix-assisted)(nanowire-assisted)laser desorption/ionization and electrospray ionization mass spectrometry // Analytical Methods. 2017. Vol. 9. No. 45. pp. 6335-6340.

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Topolyan A. P., Belyaeva M. A., Slyundina M. S., Ilyushenkova V. V., Formanovsky A. A., Korshun V. A., Borisov R. S. A novel trityl/acridine derivatization agent for analysis of thiols by (matrix-assisted)(nanowire-assisted)laser desorption/ionization and electrospray ionization mass spectrometry // Analytical Methods. 2017. Vol. 9. No. 45. pp. 6335-6340.

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TY - JOUR

DO - 10.1039/c7ay01965c

UR - https://xlink.rsc.org/?DOI=C7AY01965C

TI - A novel trityl/acridine derivatization agent for analysis of thiols by (matrix-assisted)(nanowire-assisted)laser desorption/ionization and electrospray ionization mass spectrometry

T2 - Analytical Methods

AU - Topolyan, A. P.

AU - Belyaeva, Maria A

AU - Slyundina, Mariya S

AU - Ilyushenkova, Valentina V

AU - Formanovsky, Andrey A.

AU - Korshun, Vladimir A.

AU - Borisov, Roman S.

PY - 2017

DA - 2017/10/30

PB - Royal Society of Chemistry (RSC)

SP - 6335-6340

IS - 45

VL - 9

SN - 1759-9660

SN - 1759-9679

ER -

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@article{2017_Topolyan,

author = {A. P. Topolyan and Maria A Belyaeva and Mariya S Slyundina and Valentina V Ilyushenkova and Andrey A. Formanovsky and Vladimir A. Korshun and Roman S. Borisov},

title = {A novel trityl/acridine derivatization agent for analysis of thiols by (matrix-assisted)(nanowire-assisted)laser desorption/ionization and electrospray ionization mass spectrometry},

journal = {Analytical Methods},

year = {2017},

volume = {9},

publisher = {Royal Society of Chemistry (RSC)},

month = {oct},

url = {https://xlink.rsc.org/?DOI=C7AY01965C},

number = {45},

pages = {6335--6340},

doi = {10.1039/c7ay01965c}

}

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Topolyan, A. P., et al. “A novel trityl/acridine derivatization agent for analysis of thiols by (matrix-assisted)(nanowire-assisted)laser desorption/ionization and electrospray ionization mass spectrometry.” Analytical Methods, vol. 9, no. 45, Oct. 2017, pp. 6335-6340. https://xlink.rsc.org/?DOI=C7AY01965C.