Open Access
Open access
volume 10 issue 44 pages 26022-26033

The impact of alicyclic substituents on the extraction ability of new family of 1,10-phenanthroline-2,9-diamides

Pavel S. Lemport 1, 2, 3, 4, 5
Petr I Matveev 1, 2, 3, 4, 5
Alexandr Yatsenko 1, 2, 3, 4, 5
M V Evsiunina 1, 2, 3, 4, 5
Valentine S Petrov 1, 2, 3, 4, 5
B.N. Tarasevich 1, 2, 3, 4, 5
Vitaly A Roznyatovsky 1, 2, 3, 4, 5
Pavel Dorovatovskii 5, 6, 7
Victor N. Khrustalev 5, 8, 9, 10, 11, 12
Sergey S Zhokhov 1, 2, 3, 4, 5
V. Solov'ev 5, 13, 14, 15
Leonid A. Aslanov 1, 2, 3, 4, 5
Vladimir G Petrov 1, 2, 3, 4, 5
Valentine G. Nenajdenko 1, 2, 3, 4, 5
Yu.A. Ustynyuk 1, 2, 3, 4, 5
Publication typeJournal Article
Publication date2020-07-10
scimago Q1
wos Q2
SJR0.777
CiteScore7.6
Impact factor4.6
ISSN20462069
PubMed ID:  35519740
General Chemistry
General Chemical Engineering
Abstract
Development of efficient extractants for the separation of actinides and lanthanides in the technologies of nuclear fuel cycle is one of the most urgent and complex tasks in modern nuclear energetics. New family of 4,7-dichloro-1,10-phenanthroline-2,9-dicarboxylic acid diamides based on cyclic amines was synthesized and shown to exhibit high selectivity in the La/Am pair separation (SF (Am/La ≈ 10)) and in the Am/Eu pair separation (SF (Am/Eu ≈ 12)). It was shown that pyrrolidine derived diamide is more efficient extractant for americium, curium and lanthanides from highly acidic HNO3 solution than its non-cyclic N,N,N',N'-tetraalkyl analogues. The structures of synthesized compounds were studied in details by IR, NMR spectroscopy, and single crystal X-ray diffraction. According to spectroscopy data, incorporation of aromatic rings to the amide fragment of ligand leads to complex dynamic behavior in solutions what is believed to strongly affect the extraction ability of synthesized ligands.
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GOST Copy
Lemport P. S. et al. The impact of alicyclic substituents on the extraction ability of new family of 1,10-phenanthroline-2,9-diamides // RSC Advances. 2020. Vol. 10. No. 44. pp. 26022-26033.
GOST all authors (up to 50) Copy
Lemport P. S. et al. The impact of alicyclic substituents on the extraction ability of new family of 1,10-phenanthroline-2,9-diamides // RSC Advances. 2020. Vol. 10. No. 44. pp. 26022-26033.
RIS |
Cite this
RIS Copy
TY - JOUR
DO - 10.1039/d0ra05182a
UR - https://xlink.rsc.org/?DOI=D0RA05182A
TI - The impact of alicyclic substituents on the extraction ability of new family of 1,10-phenanthroline-2,9-diamides
T2 - RSC Advances
AU - Lemport, Pavel S.
AU - Matveev, Petr I
AU - Yatsenko, Alexandr
AU - Evsiunina, M V
AU - Petrov, Valentine S
AU - Tarasevich, B.N.
AU - Roznyatovsky, Vitaly A
AU - Dorovatovskii, Pavel
AU - Khrustalev, Victor N.
AU - Zhokhov, Sergey S
AU - Solov'ev, V.
AU - Aslanov, Leonid A.
AU - Petrov, Vladimir G
AU - Kalmykov, Stepan N.
AU - Nenajdenko, Valentine G.
AU - Ustynyuk, Yu.A.
PY - 2020
DA - 2020/07/10
PB - Royal Society of Chemistry (RSC)
SP - 26022-26033
IS - 44
VL - 10
PMID - 35519740
SN - 2046-2069
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2020_Lemport,
author = {Pavel S. Lemport and Petr I Matveev and Alexandr Yatsenko and M V Evsiunina and Valentine S Petrov and B.N. Tarasevich and Vitaly A Roznyatovsky and Pavel Dorovatovskii and Victor N. Khrustalev and Sergey S Zhokhov and V. Solov'ev and Leonid A. Aslanov and Vladimir G Petrov and Stepan N. Kalmykov and Valentine G. Nenajdenko and Yu.A. Ustynyuk and others},
title = {The impact of alicyclic substituents on the extraction ability of new family of 1,10-phenanthroline-2,9-diamides},
journal = {RSC Advances},
year = {2020},
volume = {10},
publisher = {Royal Society of Chemistry (RSC)},
month = {jul},
url = {https://xlink.rsc.org/?DOI=D0RA05182A},
number = {44},
pages = {26022--26033},
doi = {10.1039/d0ra05182a}
}
MLA
Cite this
MLA Copy
Lemport, Pavel S., et al. “The impact of alicyclic substituents on the extraction ability of new family of 1,10-phenanthroline-2,9-diamides.” RSC Advances, vol. 10, no. 44, Jul. 2020, pp. 26022-26033. https://xlink.rsc.org/?DOI=D0RA05182A.