Synthesis and catalytic activity of palladium complexes bearing N-heterocyclic carbenes (NHCs) and 1,4,7-triaza-9-phosphatricyclo[5.3.2.1]tridecane (CAP) ligands
Thomas Scattolin
1
,
Vladislav A. Voloshkin
1, 2, 3, 4, 5
,
Ekaterina A Martynova
1, 2, 3, 4, 5
,
Sofie M P Vanden Broeck
1, 2, 3, 4, 5
,
Marek Beliš
1, 2, 3, 4, 5
,
Catherine S. J. Cazin
1, 2, 3, 4, 5
,
Steven P. Nolan
1, 2, 3, 4, 5
2
Department of Chemistry and Center for Sustainable Chemistry
4
Ghent
|
5
BELGIUM
|
Publication type: Journal Article
Publication date: 2021-06-14
scimago Q2
wos Q1
SJR: 0.653
CiteScore: 6.0
Impact factor: 3.3
ISSN: 14779226, 14779234
PubMed ID:
34254628
Inorganic Chemistry
Abstract
The synthesis and characterization of novel palladium complexes bearing N-heterocyclic carbenes (NHCs) and 1,4,7-triaza-9-phosphatricyclo[5.3.2.1]tridecane (CAP) are reported. These organometallic complexes can be easily obtained using two different synthetic strategies that involve either the substitution of the pyridine ligand from trans-[Pd(NHC)(Py)Cl2] or by simple addition of the CAP ligand to dimeric species [Pd(NHC)Cl2]2. The mixed NHC/CAP complexes were tested as pre-catalysts in the Buchwald–Hartwig aryl amination coupling, showing good catalytic activity, especially in the case of cis-[Pd(IPr)(CAP)Cl2].
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Scattolin T. et al. Synthesis and catalytic activity of palladium complexes bearing N-heterocyclic carbenes (NHCs) and 1,4,7-triaza-9-phosphatricyclo[5.3.2.1]tridecane (CAP) ligands // Dalton Transactions. 2021. Vol. 50. No. 27. pp. 9491-9499.
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Scattolin T., Voloshkin V. A., Martynova E. A., Vanden Broeck S. M. P., Beliš M., Cazin C. S. J., Nolan S. P. Synthesis and catalytic activity of palladium complexes bearing N-heterocyclic carbenes (NHCs) and 1,4,7-triaza-9-phosphatricyclo[5.3.2.1]tridecane (CAP) ligands // Dalton Transactions. 2021. Vol. 50. No. 27. pp. 9491-9499.
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RIS
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TY - JOUR
DO - 10.1039/d1dt01716k
UR - https://xlink.rsc.org/?DOI=D1DT01716K
TI - Synthesis and catalytic activity of palladium complexes bearing N-heterocyclic carbenes (NHCs) and 1,4,7-triaza-9-phosphatricyclo[5.3.2.1]tridecane (CAP) ligands
T2 - Dalton Transactions
AU - Scattolin, Thomas
AU - Voloshkin, Vladislav A.
AU - Martynova, Ekaterina A
AU - Vanden Broeck, Sofie M P
AU - Beliš, Marek
AU - Cazin, Catherine S. J.
AU - Nolan, Steven P.
PY - 2021
DA - 2021/06/14
PB - Royal Society of Chemistry (RSC)
SP - 9491-9499
IS - 27
VL - 50
PMID - 34254628
SN - 1477-9226
SN - 1477-9234
ER -
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BibTex (up to 50 authors)
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@article{2021_Scattolin,
author = {Thomas Scattolin and Vladislav A. Voloshkin and Ekaterina A Martynova and Sofie M P Vanden Broeck and Marek Beliš and Catherine S. J. Cazin and Steven P. Nolan},
title = {Synthesis and catalytic activity of palladium complexes bearing N-heterocyclic carbenes (NHCs) and 1,4,7-triaza-9-phosphatricyclo[5.3.2.1]tridecane (CAP) ligands},
journal = {Dalton Transactions},
year = {2021},
volume = {50},
publisher = {Royal Society of Chemistry (RSC)},
month = {jun},
url = {https://xlink.rsc.org/?DOI=D1DT01716K},
number = {27},
pages = {9491--9499},
doi = {10.1039/d1dt01716k}
}
Cite this
MLA
Copy
Scattolin, Thomas, et al. “Synthesis and catalytic activity of palladium complexes bearing N-heterocyclic carbenes (NHCs) and 1,4,7-triaza-9-phosphatricyclo[5.3.2.1]tridecane (CAP) ligands.” Dalton Transactions, vol. 50, no. 27, Jun. 2021, pp. 9491-9499. https://xlink.rsc.org/?DOI=D1DT01716K.