volume 20 issue 9 pages 1926-1932

Direct C-H borylation of vinylporphyrins via copper catalysis

Grigory L Kozhemyakin 1, 2
Victoria V Frolova 1, 2
Ivan S. Lonin 1, 2
Gelii V. Ponomarev 3, 4
Aleksey K Buryak 1, 2
Publication typeJournal Article
Publication date2022-02-10
scimago Q2
wos Q2
SJR0.600
CiteScore5.2
Impact factor2.7
ISSN14770520, 14770539
PubMed ID:  35166755
Organic Chemistry
Biochemistry
Physical and Theoretical Chemistry
Abstract
A method of direct borylation of vinyl-substituted porphyrinoids (porphyrins and chlorins) has been developed based on the copper catalyzed vinylic C-H activation. Ni(II) complexes of meso- and β-vinylporphyrinoids have been transformed to the corresponding pinacolboronated derivatives with good yields and high (E)-stereoselectivity. The method provides an easy and direct access to the valuable synthons which were shown to act as nucleophylic partners in the Suzuki cross-coupling building tetrapyrrole derivatives with π-conjugation through the carbon-carbon double bond.
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Belyaev E. S. et al. Direct C-H borylation of vinylporphyrins via copper catalysis // Organic and Biomolecular Chemistry. 2022. Vol. 20. No. 9. pp. 1926-1932.
GOST all authors (up to 50) Copy
Belyaev E. S., Kozhemyakin G. L., Tyurin V. S., Frolova V. V., Lonin I. S., Ponomarev G. V., Buryak A. K., Zamilatskov I. A. Direct C-H borylation of vinylporphyrins via copper catalysis // Organic and Biomolecular Chemistry. 2022. Vol. 20. No. 9. pp. 1926-1932.
RIS |
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RIS Copy
TY - JOUR
DO - 10.1039/d1ob02005f
UR - https://xlink.rsc.org/?DOI=D1OB02005F
TI - Direct C-H borylation of vinylporphyrins via copper catalysis
T2 - Organic and Biomolecular Chemistry
AU - Belyaev, Evgeny S.
AU - Kozhemyakin, Grigory L
AU - Tyurin, Vladimir S
AU - Frolova, Victoria V
AU - Lonin, Ivan S.
AU - Ponomarev, Gelii V.
AU - Buryak, Aleksey K
AU - Zamilatskov, Ilya A
PY - 2022
DA - 2022/02/10
PB - Royal Society of Chemistry (RSC)
SP - 1926-1932
IS - 9
VL - 20
PMID - 35166755
SN - 1477-0520
SN - 1477-0539
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2022_Belyaev,
author = {Evgeny S. Belyaev and Grigory L Kozhemyakin and Vladimir S Tyurin and Victoria V Frolova and Ivan S. Lonin and Gelii V. Ponomarev and Aleksey K Buryak and Ilya A Zamilatskov},
title = {Direct C-H borylation of vinylporphyrins via copper catalysis},
journal = {Organic and Biomolecular Chemistry},
year = {2022},
volume = {20},
publisher = {Royal Society of Chemistry (RSC)},
month = {feb},
url = {https://xlink.rsc.org/?DOI=D1OB02005F},
number = {9},
pages = {1926--1932},
doi = {10.1039/d1ob02005f}
}
MLA
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MLA Copy
Belyaev, Evgeny S., et al. “Direct C-H borylation of vinylporphyrins via copper catalysis.” Organic and Biomolecular Chemistry, vol. 20, no. 9, Feb. 2022, pp. 1926-1932. https://xlink.rsc.org/?DOI=D1OB02005F.