Mechanistic studies in the chemistry of thiourea. Part 1. Reaction with benzil under alkaline conditions
Тип публикации: Journal Article
Дата публикации: 1989-01-01
SJR: —
CiteScore: —
Impact factor: —
ISSN: 03009580, 13645471, 1472779X
General Environmental Science
General Earth and Planetary Sciences
Краткое описание
Benzil reacts under alkaline conditions with 1,3-dimethylthiourea to form 4,5-dihydroxy-1,3-dimethyl-4,5-diphenyltetrahydroimidazole-2-thione (1); with 1-methylthiourea to form 3-methyl-5,5-diphenyl-2-thiohydantoin (9); and with thiourea to form both the corresponding hydantoin and 3a,7a-diphenyltetrahydroimidazo[4,5-d]imidazole-2,5-dithione (19). The use of high field n.m.r. spectroscopy and benzil labelled with carbon-13 in the carbonyl group has permitted delineation of the reaction mechanisms and detection of a number of transient intermediates.
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ГОСТ
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Broan C. J. et al. Mechanistic studies in the chemistry of thiourea. Part 1. Reaction with benzil under alkaline conditions // Journal of the Chemical Society Perkin Transactions 2. 1989. Vol. 7. p. 731.
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Broan C. J., Butler A. R., Reed D., Sadler I. H. Mechanistic studies in the chemistry of thiourea. Part 1. Reaction with benzil under alkaline conditions // Journal of the Chemical Society Perkin Transactions 2. 1989. Vol. 7. p. 731.
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RIS
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TY - JOUR
DO - 10.1039/p29890000731
UR - https://doi.org/10.1039/p29890000731
TI - Mechanistic studies in the chemistry of thiourea. Part 1. Reaction with benzil under alkaline conditions
T2 - Journal of the Chemical Society Perkin Transactions 2
AU - Broan, Christopher J
AU - Butler, Anthony R.
AU - Reed, David
AU - Sadler, Ian H.
PY - 1989
DA - 1989/01/01
PB - Royal Society of Chemistry (RSC)
SP - 731
IS - 7
SN - 0300-9580
SN - 1364-5471
SN - 1472-779X
ER -
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BibTex (до 50 авторов)
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@article{1989_Broan,
author = {Christopher J Broan and Anthony R. Butler and David Reed and Ian H. Sadler},
title = {Mechanistic studies in the chemistry of thiourea. Part 1. Reaction with benzil under alkaline conditions},
journal = {Journal of the Chemical Society Perkin Transactions 2},
year = {1989},
publisher = {Royal Society of Chemistry (RSC)},
month = {jan},
url = {https://doi.org/10.1039/p29890000731},
number = {7},
pages = {731},
doi = {10.1039/p29890000731}
}