One-Step, Gram-Scale Synthesis of Caffeine-d9 from Xanthine and CD3I
Publication type: Journal Article
Publication date: 2022-11-04
scimago Q2
wos Q2
SJR: 0.559
CiteScore: 4.6
Impact factor: 2.3
ISSN: 00397881, 1437210X
Catalysis
Organic Chemistry
Abstract
A one-step, gram-scale synthesis of caffeine-d 9 was achieved using xanthine and CD3I. The reaction proceeds at room temperature using dimsyl sodium as base and THF as solvent, and conducting the reaction on a 1-g scale gave caffeine and caffeine-d 9 in 77% and 86% yield, respectively, after recrystallization.
Found
Nothing found, try to update filter.
Found
Nothing found, try to update filter.
Top-30
Journals
|
1
|
|
|
ChemMedChem
1 publication, 50%
|
|
|
Research on Chemical Intermediates
1 publication, 50%
|
|
|
1
|
Publishers
|
1
|
|
|
Wiley
1 publication, 50%
|
|
|
Springer Nature
1 publication, 50%
|
|
|
1
|
- We do not take into account publications without a DOI.
- Statistics recalculated weekly.
Are you a researcher?
Create a profile to get free access to personal recommendations for colleagues and new articles.
Metrics
2
Total citations:
2
Citations from 2024:
2
(100%)
Cite this
GOST |
RIS |
BibTex
Cite this
RIS
Copy
TY - JOUR
DO - 10.1055/a-1972-3819
UR - https://doi.org/10.1055/a-1972-3819
TI - One-Step, Gram-Scale Synthesis of Caffeine-d9 from Xanthine and CD3I
T2 - Synthesis
AU - Gris, Pavel
AU - Murphy, Graham J.
AU - Tarasca, Michael V
AU - Tomlinson, Cassidy J
PY - 2022
DA - 2022/11/04
PB - Georg Thieme Verlag KG
SN - 0039-7881
SN - 1437-210X
ER -
Cite this
BibTex (up to 50 authors)
Copy
@article{2022_Gris,
author = {Pavel Gris and Graham J. Murphy and Michael V Tarasca and Cassidy J Tomlinson},
title = {One-Step, Gram-Scale Synthesis of Caffeine-d9 from Xanthine and CD3I},
journal = {Synthesis},
year = {2022},
publisher = {Georg Thieme Verlag KG},
month = {nov},
url = {https://doi.org/10.1055/a-1972-3819},
doi = {10.1055/a-1972-3819}
}
Profiles