Highly Regioselective Synthesis of 3,6-Disubstituted 2-(Methylsulfanyl)pyrimidin-4(3H)-ones
Publication type: Journal Article
Publication date: 2015-09-16
scimago Q2
wos Q2
SJR: 0.559
CiteScore: 4.6
Impact factor: 2.3
ISSN: 00397881, 1437210X
Catalysis
Organic Chemistry
Abstract
This study reports a simple and highly regioselective synthesis of a new series of 3,6-disubstituted 2-(methylsulfanyl)pyrimidin-4(3H)-ones, in which the 6-substituents are methyl or aryl groups and the 3-substituents are alkyl, allyl, phenyl, benzyl, or 2-phenylethyl groups. The products are obtained in good yields by cyclocondensation of the appropriate 4-substituted 4-methoxy-1,1,1-trichloroalk-3-en-2-ones with nonsymmetric 1-substituted 2-methylisothiourea sulfates under mild basic conditions.
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dos Santos J. M. et al. Highly Regioselective Synthesis of 3,6-Disubstituted 2-(Methylsulfanyl)pyrimidin-4(3H)-ones // Synthesis. 2015. Vol. 47. No. 24. pp. 3947-3955.
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dos Santos J. M., Dos Santos J., Souza L. V. E., Lobo M. L., Bonacorso H. G., Martins M. A. P., Zanatta N. Highly Regioselective Synthesis of 3,6-Disubstituted 2-(Methylsulfanyl)pyrimidin-4(3H)-ones // Synthesis. 2015. Vol. 47. No. 24. pp. 3947-3955.
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TY - JOUR
DO - 10.1055/s-0035-1560470
UR - https://doi.org/10.1055/s-0035-1560470
TI - Highly Regioselective Synthesis of 3,6-Disubstituted 2-(Methylsulfanyl)pyrimidin-4(3H)-ones
T2 - Synthesis
AU - dos Santos, Josiane M.
AU - Dos Santos, Josiane
AU - Souza, Laura Vilela E
AU - Lobo, Marcio Luiz
AU - Bonacorso, Helio G.
AU - Martins, Marcos A. P.
AU - Zanatta, Nilo
PY - 2015
DA - 2015/09/16
PB - Georg Thieme Verlag KG
SP - 3947-3955
IS - 24
VL - 47
SN - 0039-7881
SN - 1437-210X
ER -
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@article{2015_dos Santos,
author = {Josiane M. dos Santos and Josiane Dos Santos and Laura Vilela E Souza and Marcio Luiz Lobo and Helio G. Bonacorso and Marcos A. P. Martins and Nilo Zanatta},
title = {Highly Regioselective Synthesis of 3,6-Disubstituted 2-(Methylsulfanyl)pyrimidin-4(3H)-ones},
journal = {Synthesis},
year = {2015},
volume = {47},
publisher = {Georg Thieme Verlag KG},
month = {sep},
url = {https://doi.org/10.1055/s-0035-1560470},
number = {24},
pages = {3947--3955},
doi = {10.1055/s-0035-1560470}
}
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MLA
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dos Santos, Josiane M., et al. “Highly Regioselective Synthesis of 3,6-Disubstituted 2-(Methylsulfanyl)pyrimidin-4(3H)-ones.” Synthesis, vol. 47, no. 24, Sep. 2015, pp. 3947-3955. https://doi.org/10.1055/s-0035-1560470.