An Efficient Synthesis of 3-Phosphorylated Benzoxaboroles via the Pudovik Reaction
1
Syngenta Biosciences Pvt. Ltd., Santa Monica Works
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2
Syngenta Jealott’s Hill International Research Centre
Publication type: Journal Article
Publication date: 2017-03-14
scimago Q2
wos Q2
SJR: 0.559
CiteScore: 4.6
Impact factor: 2.3
ISSN: 00397881, 1437210X
Catalysis
Organic Chemistry
Abstract
A simple, fast and efficient synthesis of 3-phosphorylated benzoxaboroles using the Pudovik reaction is reported. A number of diverse 3-(dialkoxyphosphoryl)-1-hydroxy-3H-2,1-benzoxaboroles were synthesised in 70–86% yield. Interesting hydrogen bond features were observed in the crystal lattice of the 5-chlorinated 3-bis(benzyloxy)phosphoryl derivative with both inter- and intramolecular C–H···O hydrogen bonds. Additionally, linear chains of intermolecular O–H···O hydrogen bonds were observed.
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Kamath P. et al. An Efficient Synthesis of 3-Phosphorylated Benzoxaboroles via the Pudovik Reaction // Synthesis. 2017. Vol. 49. No. 11. pp. 2435-2442.
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Kamath P., Rajan R., Deshpande S., MONTGOMERY M., Lal M. An Efficient Synthesis of 3-Phosphorylated Benzoxaboroles via the Pudovik Reaction // Synthesis. 2017. Vol. 49. No. 11. pp. 2435-2442.
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TY - JOUR
DO - 10.1055/s-0036-1588739
UR - https://doi.org/10.1055/s-0036-1588739
TI - An Efficient Synthesis of 3-Phosphorylated Benzoxaboroles via the Pudovik Reaction
T2 - Synthesis
AU - Kamath, Prashantha
AU - Rajan, Ramya
AU - Deshpande, Sudhindra
AU - MONTGOMERY, MARK
AU - Lal, Mukul
PY - 2017
DA - 2017/03/14
PB - Georg Thieme Verlag KG
SP - 2435-2442
IS - 11
VL - 49
SN - 0039-7881
SN - 1437-210X
ER -
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BibTex (up to 50 authors)
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@article{2017_Kamath,
author = {Prashantha Kamath and Ramya Rajan and Sudhindra Deshpande and MARK MONTGOMERY and Mukul Lal},
title = {An Efficient Synthesis of 3-Phosphorylated Benzoxaboroles via the Pudovik Reaction},
journal = {Synthesis},
year = {2017},
volume = {49},
publisher = {Georg Thieme Verlag KG},
month = {mar},
url = {https://doi.org/10.1055/s-0036-1588739},
number = {11},
pages = {2435--2442},
doi = {10.1055/s-0036-1588739}
}
Cite this
MLA
Copy
Kamath, Prashantha, et al. “An Efficient Synthesis of 3-Phosphorylated Benzoxaboroles via the Pudovik Reaction.” Synthesis, vol. 49, no. 11, Mar. 2017, pp. 2435-2442. https://doi.org/10.1055/s-0036-1588739.