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volume 01 issue 01 pages 143-146

Ball-Milling Promoted Monobromination Reactions: One-pot Regioselective Synthesis of Aryl Bromides and α-Bromoketones by NBS and Recyclable MCM-41-SO3H at Room Temperature

N Ghanbari
Hossein Ghafuri
H Zand
Mohammad Eslami
Publication typeJournal Article
Publication date2017-03-01
scimago Q2
wos Q3
SJR0.453
CiteScore3.6
Impact factor2.1
ISSN25099396
Catalysis
Organic Chemistry
Materials Science (miscellaneous)
Biomaterials
Abstract

An effective approach to monobromination reactions utilizing room temperature ball-milling is introduced for the synthesis of aryl bromides and bromoketones with N-bromosuccinimide (NBS) and MCM-41-SO3H. Advantages of this technique are short reaction times and high regioselectivity. In contrast to other techniques using microwaves, ultrasound, or ionic liquids, handling of sensitive materials is possible and furthermore, this method has advantages over other solvent-free techniques that require a higher reaction temperature for high yield of products.

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Ghanbari N. et al. Ball-Milling Promoted Monobromination Reactions: One-pot Regioselective Synthesis of Aryl Bromides and α-Bromoketones by NBS and Recyclable MCM-41-SO3H at Room Temperature // SynOpen. 2017. Vol. 01. No. 01. pp. 143-146.
GOST all authors (up to 50) Copy
Ghanbari N., Ghafuri H., Zand H., Eslami M. Ball-Milling Promoted Monobromination Reactions: One-pot Regioselective Synthesis of Aryl Bromides and α-Bromoketones by NBS and Recyclable MCM-41-SO3H at Room Temperature // SynOpen. 2017. Vol. 01. No. 01. pp. 143-146.
RIS |
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RIS Copy
TY - JOUR
DO - 10.1055/s-0036-1590959
UR - https://doi.org/10.1055/s-0036-1590959
TI - Ball-Milling Promoted Monobromination Reactions: One-pot Regioselective Synthesis of Aryl Bromides and α-Bromoketones by NBS and Recyclable MCM-41-SO3H at Room Temperature
T2 - SynOpen
AU - Ghanbari, N
AU - Ghafuri, Hossein
AU - Zand, H
AU - Eslami, Mohammad
PY - 2017
DA - 2017/03/01
PB - Georg Thieme Verlag KG
SP - 143-146
IS - 01
VL - 01
SN - 2509-9396
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2017_Ghanbari,
author = {N Ghanbari and Hossein Ghafuri and H Zand and Mohammad Eslami},
title = {Ball-Milling Promoted Monobromination Reactions: One-pot Regioselective Synthesis of Aryl Bromides and α-Bromoketones by NBS and Recyclable MCM-41-SO3H at Room Temperature},
journal = {SynOpen},
year = {2017},
volume = {01},
publisher = {Georg Thieme Verlag KG},
month = {mar},
url = {https://doi.org/10.1055/s-0036-1590959},
number = {01},
pages = {143--146},
doi = {10.1055/s-0036-1590959}
}
MLA
Cite this
MLA Copy
Ghanbari, N., et al. “Ball-Milling Promoted Monobromination Reactions: One-pot Regioselective Synthesis of Aryl Bromides and α-Bromoketones by NBS and Recyclable MCM-41-SO3H at Room Temperature.” SynOpen, vol. 01, no. 01, Mar. 2017, pp. 143-146. https://doi.org/10.1055/s-0036-1590959.