Synlett, volume 2005, issue 19, pages 2919-2922

Lipase-Catalyzed Asymmetric Dealkoxylcarbonylation of σ-Symmetrical β-Ketodiesters and Its Application to the Synthesis of (-)-Podocarpic Acid

Manabu Node
Takahiro Katoh
Ken Ichiro Awasaguchi
Daisuke Mori
Hiroyuki Kimura
Tetsuya Kajimoto
Publication typeJournal Article
Publication date2005-10-27
Journal: Synlett
scimago Q3
wos Q3
SJR0.450
CiteScore3.4
Impact factor1.7
ISSN09365214, 14372096
Organic Chemistry
Abstract
Optically active 2,6-dimethylcyclohexanone-2-carboxylate was prepared by PLE-catalyzed dealkoxycarbonylation of σ-symmetrical β-ketodiesters, which possess quartemary carbons at α- and α'-positions. Moreover, (-)-podocarpic acid was prepared in a short sequence from 2,6-dimethylcyclohexanone-2-carboxylate.

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