Synlett, volume 2005, issue 19, pages 2919-2922

Lipase-Catalyzed Asymmetric Dealkoxylcarbonylation of σ-Symmetrical β-Ketodiesters and Its Application to the Synthesis of (-)-Podocarpic Acid

Manabu Node

Takahiro Katoh

Ken Ichiro Awasaguchi

Daisuke Mori

Hiroyuki Kimura

Tetsuya Kajimoto

Publication type: Journal Article

Publication date: 2005-10-27

Georg Thieme Verlag KG

Journal: Synlett

scimago Q3

wos Q3

SJR: 0.450

CiteScore: 3.4

Impact factor: 1.7

ISSN: 09365214, 14372096

DOI: 10.1055/s-2005-918962

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Organic Chemistry

Abstract

Optically active 2,6-dimethylcyclohexanone-2-carboxylate was prepared by PLE-catalyzed dealkoxycarbonylation of σ-symmetrical β-ketodiesters, which possess quartemary carbons at α- and α'-positions. Moreover, (-)-podocarpic acid was prepared in a short sequence from 2,6-dimethylcyclohexanone-2-carboxylate.

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Publisher

Georg Thieme Verlag KG

Journal

Synlett

scimago Q3

wos Q3

SJR

0.450

CiteScore

3.4

Impact factor

1.7

ISSN

09365214 (Print)

14372096 (Electronic)

Lipase-Catalyzed Asymmetric Dealkoxylcarbonylation of σ-Symmetrical β-Ketodiesters and Its Application to the Synthesis of (-)-Podocarpic Acid

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