Novel macrocyclic bile acid derivatives; Selective and easy binding of two cholic acid moieties at the 3-and 3'-positions
Publication type: Journal Article
Publication date: 2009-10-19
scimago Q2
wos Q2
SJR: 0.559
CiteScore: 4.6
Impact factor: 2.3
ISSN: 00397881, 1437210X
Catalysis
Organic Chemistry
Abstract
The synthesis of macrocyclic derivatives of bile acids (cholaphanes) is elaborated using the formation of ester or amide linkages at the 3α,3'α- and 24,24'-positions of lithocholic, deoxycholic or cholic acids. The conditions were found under which the selective diacylation at the 3α,3'α- and 24,24'-positions of two molecules of cholic acid by dichloroanhydrides of arene(hetarene)dicarboxylic acid proceeds in good yields without prior protection of the 7α- and 12α-hydroxy groups.
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Lukashev N. et al. Novel macrocyclic bile acid derivatives; Selective and easy binding of two cholic acid moieties at the 3-and 3'-positions // Synthesis. 2009. Vol. 24. pp. 4175-4182.
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Lukashev N., Kazantsev A., Averin A., Donez P., Baranov M., Sievänen E., Kolehmainen E., Averin A. A. Novel macrocyclic bile acid derivatives; Selective and easy binding of two cholic acid moieties at the 3-and 3'-positions // Synthesis. 2009. Vol. 24. pp. 4175-4182.
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TY - JOUR
DO - 10.1055/s-0029-1217057
UR - https://doi.org/10.1055/s-0029-1217057
TI - Novel macrocyclic bile acid derivatives; Selective and easy binding of two cholic acid moieties at the 3-and 3'-positions
T2 - Synthesis
AU - Lukashev, Nikolay
AU - Kazantsev, Alexey
AU - Averin, Alexey
AU - Donez, Pavel
AU - Baranov, Mikhail
AU - Sievänen, Elina
AU - Kolehmainen, Erkki
AU - Averin, Alexey A
PY - 2009
DA - 2009/10/19
PB - Georg Thieme Verlag KG
SP - 4175-4182
IS - 24
SN - 0039-7881
SN - 1437-210X
ER -
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@article{2009_Lukashev,
author = {Nikolay Lukashev and Alexey Kazantsev and Alexey Averin and Pavel Donez and Mikhail Baranov and Elina Sievänen and Erkki Kolehmainen and Alexey A Averin},
title = {Novel macrocyclic bile acid derivatives; Selective and easy binding of two cholic acid moieties at the 3-and 3'-positions},
journal = {Synthesis},
year = {2009},
publisher = {Georg Thieme Verlag KG},
month = {oct},
url = {https://doi.org/10.1055/s-0029-1217057},
number = {24},
pages = {4175--4182},
doi = {10.1055/s-0029-1217057}
}
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