Georg Thieme Verlag KG
Synlett
,  volume 2010 ,  issue 14 ,  pages 2071-2074

Synthesis of Novel Allocolchicine Analogues with a Pyridine C-Ring through Intermolecular Vollhardt Diyne-Nitrile Cyclotrimerization

Hans-Günther Schmalz
, 
H.-G. Schmalz
Publication type: Journal Article
Publication date: 2010-07-22
Georg Thieme Verlag KG
scimago Q3
wos Q3
SJR: 0.437
CiteScore: 3.3
Impact factor: 1.4
ISSN: 09365214, 14372096
Organic Chemistry
Abstract
A short synthesis of new allocolchicinoids with a pyridine C-ring and an oxa-B-ring was developed exploiting a cobalt-catalyzed intermolecular [2+2+2] cycloaddition (diyne-nitrile cyclotrimerization). Starting from readily accessible 3,4,5-trimethoxybenzaldehyde or 3,4,5-trimethoxyacetophenone, the (racemic) target compounds were regioselectively obtained in 15-20% overall yield (five steps).
Found 
Found 
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GOST |
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GOST Copy
Schmalz H., Schmalz H. Synthesis of Novel Allocolchicine Analogues with a Pyridine C-Ring through Intermolecular Vollhardt Diyne-Nitrile Cyclotrimerization // Synlett. 2010. Vol. 2010. No. 14. pp. 2071-2074.
GOST all authors (up to 50) Copy
Schmalz H., Schmalz H. Synthesis of Novel Allocolchicine Analogues with a Pyridine C-Ring through Intermolecular Vollhardt Diyne-Nitrile Cyclotrimerization // Synlett. 2010. Vol. 2010. No. 14. pp. 2071-2074.
RIS |
Cite this
RIS Copy
TY - JOUR
DO - 10.1055/s-0030-1258512
UR - https://doi.org/10.1055/s-0030-1258512
TI - Synthesis of Novel Allocolchicine Analogues with a Pyridine C-Ring through Intermolecular Vollhardt Diyne-Nitrile Cyclotrimerization
T2 - Synlett
AU - Schmalz, Hans-Günther
AU - Schmalz, H.-G.
PY - 2010
DA - 2010/07/22
PB - Georg Thieme Verlag KG
SP - 2071-2074
IS - 14
VL - 2010
SN - 0936-5214
SN - 1437-2096
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2010_Schmalz,
author = {Hans-Günther Schmalz and H.-G. Schmalz},
title = {Synthesis of Novel Allocolchicine Analogues with a Pyridine C-Ring through Intermolecular Vollhardt Diyne-Nitrile Cyclotrimerization},
journal = {Synlett},
year = {2010},
volume = {2010},
publisher = {Georg Thieme Verlag KG},
month = {jul},
url = {https://doi.org/10.1055/s-0030-1258512},
number = {14},
pages = {2071--2074},
doi = {10.1055/s-0030-1258512}
}
MLA
Cite this
MLA Copy
Schmalz, Hans-Günther, and H.-G. Schmalz. “Synthesis of Novel Allocolchicine Analogues with a Pyridine C-Ring through Intermolecular Vollhardt Diyne-Nitrile Cyclotrimerization.” Synlett, vol. 2010, no. 14, Jul. 2010, pp. 2071-2074. https://doi.org/10.1055/s-0030-1258512.