Synthesis

, том 47 , издание 09 , страницы 1329-1336

Base-Catalyzed Addition of Ketones to Alkynes as a Key Step in the One-Pot Synthesis of 1-Formyl-2-pyrazolines

Тип публикации: Journal Article

Дата публикации: 2015-02-24

Georg Thieme Verlag KG

Synthesis

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SJR: 0.559

CiteScore: 4.6

Impact factor: 2.3

ISSN: 00397881, 1437210X

DOI: 10.1055/s-0034-1378687

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Catalysis

Organic Chemistry

Краткое описание

The reaction of ketones with alkynes in the presence of potassium tert -butoxide and dimethylsulfoxide followed by the treatment of the reaction mixture with hydrazine hydrate and formic acid leads to 2-pyrazoline-1-carbaldehydes in up to 81% yield.

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Schmidt E. Yu. et al. Base-Catalyzed Addition of Ketones to Alkynes as a Key Step in the One-Pot Synthesis of 1-Formyl-2-pyrazolines // Synthesis. 2015. Vol. 47. No. 09. pp. 1329-1336.

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Schmidt E. Yu., Ivanova E., Ivanova E., Semenova N. V., Ushakov I., Trofimov B. A. Base-Catalyzed Addition of Ketones to Alkynes as a Key Step in the One-Pot Synthesis of 1-Formyl-2-pyrazolines // Synthesis. 2015. Vol. 47. No. 09. pp. 1329-1336.

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TY - JOUR

DO - 10.1055/s-0034-1378687

UR - https://doi.org/10.1055/s-0034-1378687

TI - Base-Catalyzed Addition of Ketones to Alkynes as a Key Step in the One-Pot Synthesis of 1-Formyl-2-pyrazolines

T2 - Synthesis

AU - Schmidt, Elena Yu

AU - Ivanova, Elena

AU - Semenova, N. V.

AU - Ushakov, Igor

AU - Trofimov, B. A.

PY - 2015

DA - 2015/02/24

PB - Georg Thieme Verlag KG

SP - 1329-1336

IS - 09

VL - 47

SN - 0039-7881

SN - 1437-210X

ER -

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@article{2015_Schmidt,

author = {Elena Yu Schmidt and Elena Ivanova and Elena Ivanova and N. V. Semenova and Igor Ushakov and B. A. Trofimov},

title = {Base-Catalyzed Addition of Ketones to Alkynes as a Key Step in the One-Pot Synthesis of 1-Formyl-2-pyrazolines},

journal = {Synthesis},

year = {2015},

volume = {47},

publisher = {Georg Thieme Verlag KG},

month = {feb},

url = {https://doi.org/10.1055/s-0034-1378687},

number = {09},

pages = {1329--1336},

doi = {10.1055/s-0034-1378687}

}

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Schmidt, Elena Yu., et al. “Base-Catalyzed Addition of Ketones to Alkynes as a Key Step in the One-Pot Synthesis of 1-Formyl-2-pyrazolines.” Synthesis, vol. 47, no. 09, Feb. 2015, pp. 1329-1336. https://doi.org/10.1055/s-0034-1378687.