Zirconium-Catalyzed Reactions of 1-Alkynyl Phosphine Oxides and Sulfides with Et3Al
Publication type: Journal Article
Publication date: 2016-08-04
scimago Q3
wos Q3
SJR: 0.437
CiteScore: 3.3
Impact factor: 1.4
ISSN: 09365214, 14372096
Organic Chemistry
Abstract
The interaction of 1-alkynyl phosphine oxides, sulfides, and selenides with Me 3 Al and Et 3 Al under zirconocene catalysis was studied. It has been found that the pathway of the reaction of 1-alkynyl phosphine derivatives with Et 3 Al strongly depends on the nature of the substrate and the solvent. The ethylalumination takes place in the case of 1-alkynyl phosphine oxides in hexane solvent. The reaction of 1-hexynyl phosphine oxide with Et 3 Al failed when dichloromethane was used as a solvent. Zirconium-catalyzed reaction of 1-heptynyl phosphine sulfide with Et 3 Al proceeds as the cycloalumination followed by the desulfurization under the action of low-valent zirconium complexes. 1-Heptynyl phosphine selenide was subjected to full deselenation under the reaction conditions.
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Ramazanov I. R. et al. Zirconium-Catalyzed Reactions of 1-Alkynyl Phosphine Oxides and Sulfides with Et3Al // Synlett. 2016. Vol. 27. No. 18. pp. 2567-2570.
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Ramazanov I. R., Kadikova R. N., Saitova Z., Nadrshina Z., Dzhemilev U. M. Zirconium-Catalyzed Reactions of 1-Alkynyl Phosphine Oxides and Sulfides with Et3Al // Synlett. 2016. Vol. 27. No. 18. pp. 2567-2570.
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TY - JOUR
DO - 10.1055/s-0035-1562736
UR - https://doi.org/10.1055/s-0035-1562736
TI - Zirconium-Catalyzed Reactions of 1-Alkynyl Phosphine Oxides and Sulfides with Et3Al
T2 - Synlett
AU - Ramazanov, Ilfir R
AU - Kadikova, Rita N.
AU - Saitova, Zukhra
AU - Nadrshina, Zifa
AU - Dzhemilev, Usein M
PY - 2016
DA - 2016/08/04
PB - Georg Thieme Verlag KG
SP - 2567-2570
IS - 18
VL - 27
SN - 0936-5214
SN - 1437-2096
ER -
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@article{2016_Ramazanov,
author = {Ilfir R Ramazanov and Rita N. Kadikova and Zukhra Saitova and Zifa Nadrshina and Usein M Dzhemilev},
title = {Zirconium-Catalyzed Reactions of 1-Alkynyl Phosphine Oxides and Sulfides with Et3Al},
journal = {Synlett},
year = {2016},
volume = {27},
publisher = {Georg Thieme Verlag KG},
month = {aug},
url = {https://doi.org/10.1055/s-0035-1562736},
number = {18},
pages = {2567--2570},
doi = {10.1055/s-0035-1562736}
}
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MLA
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Ramazanov, Ilfir R., et al. “Zirconium-Catalyzed Reactions of 1-Alkynyl Phosphine Oxides and Sulfides with Et3Al.” Synlett, vol. 27, no. 18, Aug. 2016, pp. 2567-2570. https://doi.org/10.1055/s-0035-1562736.