Hypervalent Iodine Mediated Efficient Solvent-Free Regioselective Halogenation and Thiocyanation of Fused N-Heterocycles
Publication type: Journal Article
Publication date: 2019-06-12
scimago Q3
wos Q3
SJR: 0.437
CiteScore: 3.3
Impact factor: 1.4
ISSN: 09365214, 14372096
Organic Chemistry
Abstract
A facile, rapid, metal-free regioselective halogenation and thiocyanation of imidazo[1,2-a]pyridine/pyrimidine heterocycles has been achieved under solvent-free reaction conditions. Halogenations and thiocyanation of the heterocycles could be accomplished by simple grinding of reactants and hypervalent iodine reagents with the corresponding alkali metal or ammonium salts. The method has been extrapolated to a cleaner synthesis of brominated imidazo[1,2-a]pyridine/pyrimidine derivatives, starting from the corresponding heterocyclic amines and substituted α-bromoketones, utilising HBr generated in situ as the source of bromine.
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GOST
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Indukuri D. R. et al. Hypervalent Iodine Mediated Efficient Solvent-Free Regioselective Halogenation and Thiocyanation of Fused N-Heterocycles // Synlett. 2019. Vol. 30. No. 13. pp. 1573-1579.
GOST all authors (up to 50)
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Indukuri D. R., Potuganti G. R., Alla M. Hypervalent Iodine Mediated Efficient Solvent-Free Regioselective Halogenation and Thiocyanation of Fused N-Heterocycles // Synlett. 2019. Vol. 30. No. 13. pp. 1573-1579.
Cite this
RIS
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TY - JOUR
DO - 10.1055/s-0037-1611856
UR - https://doi.org/10.1055/s-0037-1611856
TI - Hypervalent Iodine Mediated Efficient Solvent-Free Regioselective Halogenation and Thiocyanation of Fused N-Heterocycles
T2 - Synlett
AU - Indukuri, Divakar Reddy
AU - Potuganti, Gal Reddy
AU - Alla, Manjula
PY - 2019
DA - 2019/06/12
PB - Georg Thieme Verlag KG
SP - 1573-1579
IS - 13
VL - 30
SN - 0936-5214
SN - 1437-2096
ER -
Cite this
BibTex (up to 50 authors)
Copy
@article{2019_Indukuri,
author = {Divakar Reddy Indukuri and Gal Reddy Potuganti and Manjula Alla},
title = {Hypervalent Iodine Mediated Efficient Solvent-Free Regioselective Halogenation and Thiocyanation of Fused N-Heterocycles},
journal = {Synlett},
year = {2019},
volume = {30},
publisher = {Georg Thieme Verlag KG},
month = {jun},
url = {https://doi.org/10.1055/s-0037-1611856},
number = {13},
pages = {1573--1579},
doi = {10.1055/s-0037-1611856}
}
Cite this
MLA
Copy
Indukuri, Divakar Reddy, et al. “Hypervalent Iodine Mediated Efficient Solvent-Free Regioselective Halogenation and Thiocyanation of Fused N-Heterocycles.” Synlett, vol. 30, no. 13, Jun. 2019, pp. 1573-1579. https://doi.org/10.1055/s-0037-1611856.