Direct Evidence for Bidentate Character of Potentially Tridentate N,S-Ligands. Molecular Structures of Bis[N-(2-pyridyl)thiosalicylidene-κS-amino-κN]nickel(II) and Bis{1-isopropyl-3-methyl-4-[N-(2-pyridyl)imino-κN-methyl]pyrazole-5-thiolato-κS}copper(II)
Publication type: Journal Article
Publication date: 1992-01-01
scimago Q3
wos Q3
SJR: 0.305
CiteScore: 3.0
Impact factor: 1.7
ISSN: 09599436, 1364551X
General Chemistry
Abstract
Two novel metal chelates with MN2S2 coordination: bis[N-(2-pyridyl)thiosalicylidene-κS-amino-κN]nickel(II) 1 and bis{1-isopropyl-3-methyl-4-[N-(2-pyridyl)imino-κN-methyl]pyrazole-5-thiolato-κS}copper(II) 2 have been investigated; both contain an additional potentially active nitrogen centre in the α-pyridyl substituents on the imino groups, but X-ray structural investigation shows that in neither case is the pyridyl nitrogen atom coordinated to the metal; complex 1 has a slightly distorted cis-planar configuration with a dihedral angle between the NNiS and N’NiS’planes of 13.5° and a shortened S S distance, 2.864(5) A, while the Cu atom in 2 has a cis-distorted tetrahedral coordination [dihedral angle between NCuS and N’CuS’ planes 57.6°, S S distance 3.178(4) A].
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Citations from 2024:
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Mistryukov A. E. et al. Direct Evidence for Bidentate Character of Potentially Tridentate N,S-Ligands. Molecular Structures of Bis[N-(2-pyridyl)thiosalicylidene-κS-amino-κN]nickel(II) and Bis{1-isopropyl-3-methyl-4-[N-(2-pyridyl)imino-κN-methyl]pyrazole-5-thiolato-κS}copper(II) // Mendeleev Communications. 1992. Vol. 2. No. 1. pp. 30-32.
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Mistryukov A. E., Vasilchenko I. S., Sergienko V. S., Nivorozhkin A. L., Kochin S. G., Porai Koshits M. A., Nivorozhkin L. E., Garnovskii A. D. Direct Evidence for Bidentate Character of Potentially Tridentate N,S-Ligands. Molecular Structures of Bis[N-(2-pyridyl)thiosalicylidene-κS-amino-κN]nickel(II) and Bis{1-isopropyl-3-methyl-4-[N-(2-pyridyl)imino-κN-methyl]pyrazole-5-thiolato-κS}copper(II) // Mendeleev Communications. 1992. Vol. 2. No. 1. pp. 30-32.
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TY - JOUR
DO - 10.1070/MC1992v002n01ABEH000112
UR - https://doi.org/10.1070/MC1992v002n01ABEH000112
TI - Direct Evidence for Bidentate Character of Potentially Tridentate N,S-Ligands. Molecular Structures of Bis[N-(2-pyridyl)thiosalicylidene-κS-amino-κN]nickel(II) and Bis{1-isopropyl-3-methyl-4-[N-(2-pyridyl)imino-κN-methyl]pyrazole-5-thiolato-κS}copper(II)
T2 - Mendeleev Communications
AU - Mistryukov, Alexander E
AU - Vasilchenko, Igor S
AU - Sergienko, Vladimir S.
AU - Nivorozhkin, Alexander L
AU - Kochin, Stanislav G
AU - Porai Koshits, Mikhail A
AU - Nivorozhkin, Leonid E
AU - Garnovskii, Alexander D
PY - 1992
DA - 1992/01/01
PB - OOO Zhurnal "Mendeleevskie Soobshcheniya"
SP - 30-32
IS - 1
VL - 2
SN - 0959-9436
SN - 1364-551X
ER -
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@article{1992_Mistryukov,
author = {Alexander E Mistryukov and Igor S Vasilchenko and Vladimir S. Sergienko and Alexander L Nivorozhkin and Stanislav G Kochin and Mikhail A Porai Koshits and Leonid E Nivorozhkin and Alexander D Garnovskii},
title = {Direct Evidence for Bidentate Character of Potentially Tridentate N,S-Ligands. Molecular Structures of Bis[N-(2-pyridyl)thiosalicylidene-κS-amino-κN]nickel(II) and Bis{1-isopropyl-3-methyl-4-[N-(2-pyridyl)imino-κN-methyl]pyrazole-5-thiolato-κS}copper(II)},
journal = {Mendeleev Communications},
year = {1992},
volume = {2},
publisher = {OOO Zhurnal "Mendeleevskie Soobshcheniya"},
month = {jan},
url = {https://doi.org/10.1070/MC1992v002n01ABEH000112},
number = {1},
pages = {30--32},
doi = {10.1070/MC1992v002n01ABEH000112}
}
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Mistryukov, Alexander E., et al. “Direct Evidence for Bidentate Character of Potentially Tridentate N,S-Ligands. Molecular Structures of Bis[N-(2-pyridyl)thiosalicylidene-κS-amino-κN]nickel(II) and Bis{1-isopropyl-3-methyl-4-[N-(2-pyridyl)imino-κN-methyl]pyrazole-5-thiolato-κS}copper(II).” Mendeleev Communications, vol. 2, no. 1, Jan. 1992, pp. 30-32. https://doi.org/10.1070/MC1992v002n01ABEH000112.
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