Regioselectivity of the substitution for the nitro group in 2,4,6-trinitrobenzonitrile under the action of thiols. The synthesis of 4,6-dinitro derivatives of benzoannelated sulfur-containing heterocycles
Тип публикации: Journal Article
Дата публикации: 2000-01-01
SCImago Q3
WOS Q3
БС1
SJR: 0.276
CiteScore: 3
Impact factor: 1.7
ISSN: 09599436, 1364551X
General Chemistry
Краткое описание
Conditions for the regioselective substitution for a nitro group in the ortho -position in 2,4,6-trinitrobenzonitrile under the action of thiols (PhCH 2 SH, HSCH 2 CO 2 Et or PhSH) in the presence of K 2 CO 3 or KOH were found, and the intramolecular cyclization of the ortho -fragments –SX and –CN (X = Cl or CH 2 CO 2 Et) was performed to afford 3-chloro-4,6-dinitrobenzo[ d ]isothiazole and 3-amino- 2-ethoxycarbonyl-4,6-dinitrobenzo[ b ]thiophene, respectively.
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Dalinger I. L. et al. Regioselectivity of the substitution for the nitro group in 2,4,6-trinitrobenzonitrile under the action of thiols. The synthesis of 4,6-dinitro derivatives of benzoannelated sulfur-containing heterocycles // Mendeleev Communications. 2000. Vol. 10. No. 2. pp. 72-73.
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Dalinger I. L., Cherkasova T. I., Khutoretskii V. M., Shevelev S. A. Regioselectivity of the substitution for the nitro group in 2,4,6-trinitrobenzonitrile under the action of thiols. The synthesis of 4,6-dinitro derivatives of benzoannelated sulfur-containing heterocycles // Mendeleev Communications. 2000. Vol. 10. No. 2. pp. 72-73.
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TY - JOUR
DO - 10.1070/mc2000v010n02abeh001220
UR - https://doi.org/10.1070/mc2000v010n02abeh001220
TI - Regioselectivity of the substitution for the nitro group in 2,4,6-trinitrobenzonitrile under the action of thiols. The synthesis of 4,6-dinitro derivatives of benzoannelated sulfur-containing heterocycles
T2 - Mendeleev Communications
AU - Dalinger, Igor L
AU - Cherkasova, Tatyana I
AU - Khutoretskii, Valerian M
AU - Shevelev, Svyatoslav A.
PY - 2000
DA - 2000/01/01
PB - OOO Zhurnal "Mendeleevskie Soobshcheniya"
SP - 72-73
IS - 2
VL - 10
SN - 0959-9436
SN - 1364-551X
ER -
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@article{2000_Dalinger,
author = {Igor L Dalinger and Tatyana I Cherkasova and Valerian M Khutoretskii and Svyatoslav A. Shevelev},
title = {Regioselectivity of the substitution for the nitro group in 2,4,6-trinitrobenzonitrile under the action of thiols. The synthesis of 4,6-dinitro derivatives of benzoannelated sulfur-containing heterocycles},
journal = {Mendeleev Communications},
year = {2000},
volume = {10},
publisher = {OOO Zhurnal "Mendeleevskie Soobshcheniya"},
month = {jan},
url = {https://doi.org/10.1070/mc2000v010n02abeh001220},
number = {2},
pages = {72--73},
doi = {10.1070/mc2000v010n02abeh001220}
}
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Dalinger, Igor L., et al. “Regioselectivity of the substitution for the nitro group in 2,4,6-trinitrobenzonitrile under the action of thiols. The synthesis of 4,6-dinitro derivatives of benzoannelated sulfur-containing heterocycles.” Mendeleev Communications, vol. 10, no. 2, Jan. 2000, pp. 72-73. https://doi.org/10.1070/mc2000v010n02abeh001220.
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