Crystal structure of diaqua[N,N′-bis(tetrafluoropyridyl)diaza-18- crown-6]lead(II) perchlorate: The effect of perfluoroaromatic groups on the stucture of the complex
Publication type: Journal Article
Publication date: 2006-01-01
scimago Q3
wos Q3
SJR: 0.305
CiteScore: 3.0
Impact factor: 1.7
ISSN: 09599436, 1364551X
General Chemistry
Abstract
According to X-ray analysis data, in the [PbL(H2O)2]2+ complex cation [L = N,N′-di(tetrafluoropyridyl)diaza-18-crown-6], the Pb atom is coordinated asymmetrically by four O(1)–O(4) atoms of the macrocycle and two O(5), O(6) atoms of water molecules, and, additionally, at longer distances, by the ortho-fluorine atoms F(4), F(5) of two perfluoropyridyl rings and the N(1), N(2) atoms of the macrocycle, thus demonstrating a partial localization of the lone electron pair of Pb. Using 1H NMR, the stability of the complex of L with Pb(ClO4)2 in [2H6]acetone was estimated (log β = 0.9).
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Sazonov P. K. et al. Crystal structure of diaqua[N,N′-bis(tetrafluoropyridyl)diaza-18- crown-6]lead(II) perchlorate: The effect of perfluoroaromatic groups on the stucture of the complex // Mendeleev Communications. 2006. Vol. 16. No. 3. pp. 147-149.
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Sazonov P. K., Minacheva L. Kh., Sergienko V. S., Artamkina G. A., Oprunenko Y. F., Beletskaya I. P. Crystal structure of diaqua[N,N′-bis(tetrafluoropyridyl)diaza-18- crown-6]lead(II) perchlorate: The effect of perfluoroaromatic groups on the stucture of the complex // Mendeleev Communications. 2006. Vol. 16. No. 3. pp. 147-149.
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TY - JOUR
DO - 10.1070/MC2006v016n03ABEH002323
UR - https://doi.org/10.1070/MC2006v016n03ABEH002323
TI - Crystal structure of diaqua[N,N′-bis(tetrafluoropyridyl)diaza-18- crown-6]lead(II) perchlorate: The effect of perfluoroaromatic groups on the stucture of the complex
T2 - Mendeleev Communications
AU - Sazonov, Petr K
AU - Minacheva, Lidiya Kh
AU - Sergienko, Vladimir S.
AU - Artamkina, Galina A.
AU - Oprunenko, Yurii F
AU - Beletskaya, Irina P.
PY - 2006
DA - 2006/01/01
PB - OOO Zhurnal "Mendeleevskie Soobshcheniya"
SP - 147-149
IS - 3
VL - 16
SN - 0959-9436
SN - 1364-551X
ER -
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@article{2006_Sazonov,
author = {Petr K Sazonov and Lidiya Kh Minacheva and Vladimir S. Sergienko and Galina A. Artamkina and Yurii F Oprunenko and Irina P. Beletskaya},
title = {Crystal structure of diaqua[N,N′-bis(tetrafluoropyridyl)diaza-18- crown-6]lead(II) perchlorate: The effect of perfluoroaromatic groups on the stucture of the complex},
journal = {Mendeleev Communications},
year = {2006},
volume = {16},
publisher = {OOO Zhurnal "Mendeleevskie Soobshcheniya"},
month = {jan},
url = {https://doi.org/10.1070/MC2006v016n03ABEH002323},
number = {3},
pages = {147--149},
doi = {10.1070/MC2006v016n03ABEH002323}
}
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MLA
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Sazonov, Petr K., et al. “Crystal structure of diaqua[N,N′-bis(tetrafluoropyridyl)diaza-18- crown-6]lead(II) perchlorate: The effect of perfluoroaromatic groups on the stucture of the complex.” Mendeleev Communications, vol. 16, no. 3, Jan. 2006, pp. 147-149. https://doi.org/10.1070/MC2006v016n03ABEH002323.