Crystal structure of diaqua[N,N′-bis(tetrafluoropyridyl)diaza-18-crown-6]lead(II) perchlorate: the effect of perfluoroaromatic groups on the stucture of the complex
Тип публикации: Journal Article
Дата публикации: 2006-07-06
SCImago Q3
WOS Q3
БС1
SJR: 0.276
CiteScore: 2.7
Impact factor: 1.4
ISSN: 09599436, 1364551X
General Chemistry
Краткое описание
According to X-ray analysis data, in the [PbL(H2O)2]2+ complex cation [L = N,N′-di(tetrafluoropyridyl)diaza-18-crown-6], the Pb atom is coordinated asymmetrically by four O(1)–O(4) atoms of the macrocycle and two O(5), O(6) atoms of water molecules, and, additionally, at longer distances, by the ortho-fluorine atoms F(4), F(5) of two perfluoropyridyl rings and the N(1), N(2) atoms of the macrocycle, thus demonstrating a partial localization of the lone electron pair of Pb. Using 1H NMR, the stability of the complex of L with Pb(ClO4)2 in [2H6]acetone was estimated (log β = 0.9).
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Sazonov P. K. et al. Crystal structure of diaqua[N,N′-bis(tetrafluoropyridyl)diaza-18-crown-6]lead(II) perchlorate: the effect of perfluoroaromatic groups on the stucture of the complex // Mendeleev Communications. 2006. Vol. 16. No. 3. pp. 147-149.
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Sazonov P. K., Minacheva L. K., Sergienko V. S., Artamkina G. A., Oprunenko Y. F., Beletskaya I. P. Crystal structure of diaqua[N,N′-bis(tetrafluoropyridyl)diaza-18-crown-6]lead(II) perchlorate: the effect of perfluoroaromatic groups on the stucture of the complex // Mendeleev Communications. 2006. Vol. 16. No. 3. pp. 147-149.
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TY - JOUR
DO - 10.1070/MC2006v016n03ABEH002323
UR - production/publications/10.1070/MC2006v016n03ABEH002323
TI - Crystal structure of diaqua[N,N′-bis(tetrafluoropyridyl)diaza-18-crown-6]lead(II) perchlorate: the effect of perfluoroaromatic groups on the stucture of the complex
T2 - Mendeleev Communications
AU - Sazonov, Petr Kirillovich
AU - Minacheva, Lidiya Khabibovna
AU - Sergienko, Vladimir Semenovich
AU - Artamkina, Galina Anisimovna
AU - Oprunenko, Yurii Fedorovich
AU - Beletskaya, Irina P.
PY - 2006
DA - 2006/07/06
PB - OOO Zhurnal "Mendeleevskie Soobshcheniya"
SP - 147-149
IS - 3
VL - 16
SN - 0959-9436
SN - 1364-551X
ER -
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@article{2006_Sazonov,
author = {Petr Kirillovich Sazonov and Lidiya Khabibovna Minacheva and Vladimir Semenovich Sergienko and Galina Anisimovna Artamkina and Yurii Fedorovich Oprunenko and Irina P. Beletskaya},
title = {Crystal structure of diaqua[N,N′-bis(tetrafluoropyridyl)diaza-18-crown-6]lead(II) perchlorate: the effect of perfluoroaromatic groups on the stucture of the complex},
journal = {Mendeleev Communications},
year = {2006},
volume = {16},
publisher = {OOO Zhurnal "Mendeleevskie Soobshcheniya"},
month = {jul},
url = {production/publications/10.1070/MC2006v016n03ABEH002323},
number = {3},
pages = {147--149},
doi = {10.1070/MC2006v016n03ABEH002323}
}
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Sazonov, Petr Kirillovich, et al. “Crystal structure of diaqua[N,N′-bis(tetrafluoropyridyl)diaza-18-crown-6]lead(II) perchlorate: the effect of perfluoroaromatic groups on the stucture of the complex.” Mendeleev Communications, vol. 16, no. 3, Jul. 2006, pp. 147-149. production/publications/10.1070/MC2006v016n03ABEH002323.
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